Engineering method for separating and extracting xanthic gum

A xanthan gum and separation process technology, applied in the engineering field of xanthan gum separation and extraction, can solve the problems of increasing the risk of explosion and fire at the production site, large fluctuations in product quality, and large consumption of organic solvents, etc., to achieve safety in the production process Reliable, saving equipment and plant investment, low production cost

Inactive Publication Date: 2004-11-17
张孝宽
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Problems solved by technology

Therefore, the consumption of organic solvent is very large, accounting for about 25-40% of the production cost, and some production enterprises even reach more than 50% of the production cost.
Not only that, these organic solvents are flammable and explosive dangerous goods, and the large amount of solvent evaporation will increase the risk of explosion and fire at the production site
At the same time, this intermittent and open production leads to large fluctuations in product quality, poor production environment, low efficiency, and high labor intensity.
Although the direct drying method and the enzyme-ultrafiltration-direct drying method can avoid the above problems, the products contain more impurities and poor quality, and their use is limited to a certain extent

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  • Engineering method for separating and extracting xanthic gum

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Embodiment Construction

[0013] Such as figure 1 As shown, the pretreated fermentation broth is first passed through the membrane filtration device 1, and concentrated by ultrafiltration using membrane separation technology to remove part of the water and impurities; then in the first unit 2, it is mixed and precipitated with an organic solvent instantaneously, and the pH is adjusted at the same time. Value; After separating the filtrate, enter the second unit 3, and then perform a mixing, precipitation and separation operation. In order to reduce the consumption of organic solvent, the filtrate of the second unit 3 can be returned to the first unit 2 to mix with xanthan gum.

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Abstract

The engineering method for separating and extracting xanthan gum is characterized by that the processes of charging materials, mixing, precipitation, separation and regulation of pH value can be continuously uniformly implemented in a closed mechanical equipment. Said ivnention can maximally prevent the organic solvent from producing volatillization in the course of production, under the normal production condition does not produce explosive gas, and can ensure safe production. As compared with ethyl alcohol precipitation method its alcohol consumption can be reduced by 80%, if after extraction vacuum drying process is adopted the ethyl alcohol consumption can be reduced by 95%. Its product quality is high and stable.

Description

1. Technical field [0001] The invention provides a new engineering method for separating and extracting xanthan gum. This method is applicable to many different xanthan gum extraction processes. 2. Background technology [0002] Xanthan gum (Xanthan gum) is an extracellular acidic heteropolysaccharide produced by the fermentation of Xanthomonas campestris, also known as xanthomonas polysaccharide. As early as 1958, Lilly et al. in the United States had isolated a strain of Xanthomonas phaseolus, which could convert starch into water-soluble viscous polysaccharides. The Peoria laboratory in the northern region of the United States Department of Agriculture first obtained xanthan gum by microbial fermentation in the early 1960s. In 1961, Kelco Company of the United States started semi-industrial production of xanthan gum using Xanthomonas campestris NRRLB-1459, which was mainly used for drilling mud and oil recovery technology of oil wells. It was officially industrialized i...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08B37/00
Inventor 张孝宽张岩
Owner 张孝宽
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