Method for preparing nano tube of some metalloid oxides and metals with size and shape being controllable
An amphoteric metal, metal nanotechnology, used in oxide/hydroxide preparation, nanotechnology for materials and surface science, nanostructure fabrication, etc.
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[0007] Preparation of Cu nanotubes: 1mmol CuCl 2 ·H 2 O was dissolved in 5ml deionized water, then, this solution was slowly added dropwise to 130ml NaOH(3M) solution, stirred well, and then 3mmol C was added 16 TMABr (hexadecyl trimethyl amine bromide, condensed to CTAB), stir well at 40-50 ℃ until the surfactant is completely dissolved, a clear and transparent solution is obtained, and 1ml of hydrazine hydrate (N 2 H 4 ) Solution, the homogeneous solution obtained by stirring is further reacted at 20-70°C for 3-7 hours to obtain a dark red precipitate. The product is separated by centrifugation, and washed repeatedly with absolute ethanol and deionized water for 5-8 times to make the surface active The agent and other inorganic ions are completely removed, and then the precipitate is separated by centrifugation, and dried under vacuum at room temperature for 4-5 hours to obtain the product Cu nanotubes with a yield of 95% (calculated as Cu).
[0008] Cu 2 Preparation of O nanotu...
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