Chinese medicine composition and its prepn process and quality control method
A quality control method and composition technology, which is applied in the direction of drug combination, testing of pharmaceutical preparations, pharmaceutical formulations, etc., and can solve problems such as lack of clear positioning
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Embodiment 1
[0043] Prescription: Fermented Cordyceps Fungus Powder 100g, American Ginseng 200g
[0044] Preparation method: The above two flavors, American ginseng are crushed into fine powder, mixed with fermented Cordyceps fungus powder, put into capsules, and made into 1000 capsules.
[0045]Identification: 1) Take 1 g of the content of this product, add 10 ml of ethanol, ultrasonically treat it for 20 minutes, filter, and use the filtrate as the test solution. Another 0.6 g of fermented Cordyceps fungus powder control medicinal material was taken, and the control medicinal material solution was prepared by the same method. According to the thin-layer chromatography test, draw 6 μl of each of the above two solutions, point them on the same silica gel G thin-layer plate, use cyclohexane-acetone (2:1) as the developing solvent, develop, take out, dry in the air, and set the UV Viewed under light (365nm). In the chromatogram of the test substance, there are fluorescent spots of the same...
Embodiment 2
[0054] Prescription: Fermented Cordyceps Fungus Powder 400g, American Ginseng 200g
[0055] Preparation method: For the above two flavors, American ginseng is crushed into fine powder, mixed with fermented Cordyceps fungus powder, add 100g of microcrystalline cellulose, add starch to a total of 1000g, mix well, use water to make soft material, and make pellets by mechanism method , dried, packaged and ready to use.
[0056] Identification: (1) Take this product, pulverize it into fine powder, weigh 2g, add 20ml of ethanol, ultrasonically treat for 20 minutes, filter, evaporate the filtrate to dryness in a water bath, add 2ml of ethanol to the residue to dissolve it, and use it as the test solution. Take another adenine reference substance, adenosine reference substance and uridine reference substance, add diluted ethanol to make a reference substance solution containing 0.5mg per 1ml. According to the thin-layer chromatography test, draw 5 μl of each of the above two solution...
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