Method and apparatus for production of bio-ethanol and other fermentation products
a technology of bioethanol and other fermentation products, applied in the direction of biofuels, biochemistry apparatus and processes, fermentation, etc., can solve the problems of affecting economic growth, affecting the market for upgraded by-products, and not being able to match the production market, so as to increase the amount of solid-state materials, increase the conversion rate, and increase the production capacity
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example 1
Illustrative Example 1
[0254]Anaerobic digested sewage sludge below was converted according to the method of the present invention in the laboratory scale plant shown in FIG. 1.
[0255]The dry matter content of the sewage sludge was 5%. The main components of the dry matter in weight % were:[0256]C=28.3%[0257]H=4.33%[0258]N=3.55%[0259]O=28.4%[0260]P=4.49%[0261]Al=7.77%[0262]Si=7.44%[0263]Ca=6.95%[0264]Fe=3.17%[0265]K=1.62%
[0266]An elemental analysis of sewage sludge dry matter was further analyzed by induced coupled plasma (ICP) revealing the following composition:
C [%]O [%]Al [%]H [%]Ca [%]Si [%]N [%]P [%]K [%]30.930.56.155.25.034.984.664.622.36Cl [%]S [%]Fe [%]Na [%]Mg [%]Zn [%]Ti [%]Ba [%]Mn [%]1.131.091.040.9380.8750.2260.1950.06520.0375
[0267]The combustible fraction amounts to 58% of the dry matter content, with a heat value of 22.2 MJ / kg, which translates into a calorific value of 476 KJ / kg in the sewage sludge as received.
[0268]Prior to the test the se...
example 2
Illustrative Example 2
[0288]Anaerobic digested sewage sludge with characteristics as given above in example was preheated and converted using the same catalyst and experimental set-up.
[0289]140 g / h of the pretreated sewage sludge was pressurized to 250 bar and heated to 230 C in the pre-heating step. This stream was mixed with 414 g / h of pressurized water heated to a temperature so as to obtain a substantially constant temperature of 300±5 C after mixing.
[0290]The mixed flow was subsequently contacted with the heterogeneous catalyst in the reactor. The feed to water ratio translates into a water to feed ratio of 3:1, and the total flow of 545 g / h translates into a contact time of 3.3 minutes.
[0291]After to the contact with the heterogeneous catalyst, the fluid containing the converted organic material is cooled to ambient temperature, filtered through a particle filter for collection of suspended particles, and expanded to ambient pressure. The liquid frac...
example 3
Illustrative Example 3
Conversion of Corn Silage
[0304]Corn silage was pretreated and converted using the same catalyst and experimental set-up as described above in example 1 and 2.
[0305]Prior to the test the sewage sludge was pretreated by sizing to less than 1 mm by cutting longer particles by a Seepex macerator (type 25 / 15-I-I-F12-2) and milling by a colloid mill (Probst und Class, type N100 / E), and filtered by a screen basket filter (mesh width 1 mm).
[0306]Subsequently 1.5% by weight of potassium in the form of potassium carbonate was added to the resulting slurry. The pH value of the slurry was 9.6.
[0307]The characteristics of the corn silage after the pretreatment were the following:
Corn silage feedstockDry matter content [% weight]11.29Inorganic fraction of dry matter29.4[% Weight]Density [kg / m3]1.0099pH9.6Heat of combustion1 [kJ / kg]14351Based on 18 MJ / kg heat of combustion for the organic fraction of the dry matter.
[0308]The inorganic content of the dry matter was mainly the ...
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