Treatment liquid for plastic film, primer liquid for printing, ink composition, and method for ink jet recording using them
a technology of plastic film and treatment liquid, which is applied in the direction of inks, instruments, transportation and packaging, etc., can solve the problems of solvent volatile components, solvent-type inks, and solvent odor, and achieve the effects of improving rubbing resistance, scratch resistance, and waterfastness
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[0324]The present invention is further illustrated by the following Examples that are not intended as a limitation of the invention.
A. Treatment Liquid
Cyclic Ester Compound
A-1. Preparation of Treatment Liquids
[0325]Treatment liquids according to the present invention were prepared according to the following formulations.
[0326]Treatment Liquid 1e:[0327]γ-Butyrolactone 10.0% by weight[0328]Diethylene glycol monobutyl ether 3.0% by weight[0329]Surfynol 465 1.0% by weight[0330]Pure water Balance
[0331]Treatment Liquid 2e:[0332]Propylene carbonate 15.0% by weight[0333]Diethylene glycol monobutyl ether 3.0% by weight[0334]Surfynol 465 1.0% by weight[0335]Pure water Balance
A-2. Preparation of Water-Based Pigment Ink Compositions
[0336]Water-based pigment ink compositions were prepared according to the following formulation.
[0337]Black Ink:[0338]Carbon Black MA7 (manufactured by Mitsubishi Kasei Corp.) 5.0% by weight[0339]Styrene-acrylic acid copolymer[0340](thermoplastic resin) 2.5% by weigh...
examples a1
to A5
[0377]Treatment liquid 1e or treatment liquid 2e was coated at 50% duty onto a non-surface-treated flexible vinyl chloride film (Scotchcal Film, manufactured by Sumitomo 3M Ltd.) for ink jet printing, with an ink jet printer (TM-J8000; manufactured by Seiko Epson Corporation). Thereafter, the coated film was dried until the water was removed by evaporation in a thermostatic chamber kept at a temperature of 60° C. and a relative humidity of 20% for one min. Immediately after that, a 100% duty pattern was printed with an ink jet printer (TM-J8000; manufactured by Seiko Epson Corporation) loaded with a black ink or with a cyan ink, a magenta ink, and a yellow ink.
[0378]Printing samples were dried in a thermostatic chamber kept at a temperature of 60° C. and a relative humidity of 20% for one hr and further at room temperature for one day and were then subjected to the following evaluation tests.
Preparation of Printing Samples
Examples A6 to A9 (Comparative Examples)
[0379]Printing w...
examples b1 to b5
[0411]Treatment liquid 1e or treatment liquid 2e was coated at 50% duty onto a non-surface-treated specialty flexible vinyl chloride film (Scotchcal Film, manufactured by Sumitomo 3M Ltd.) for ink jet printing, with an ink jet printer (TM-J8000; manufactured by Seiko Epson Corporation). Thereafter, the coated film was dried until the water was removed by evaporation in a thermostatic chamber kept at a temperature of 60° C. and a relative humidity of 20% for 5 min. Immediately after that, a 100% duty pattern was printed with an ink jet printer (TM-J8000; manufactured by Seiko Epson Corporation) loaded with a black ink or with a cyan ink, a magenta ink, and a yellow ink.
[0412]Printing samples were dried in a thermostatic chamber kept at a temperature of 60° C. and a relative humidity of 20% for one hr and further at room temperature for one day and were then subjected to the following evaluation tests.
Preparation of Printing Samples
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