Water solvated glass/amorphous solid ionic conductors
a technology of amorphous solids and ionic conductors, which is applied in the manufacture of final products, calcium/strontium/barium sulfates, silicates, etc., can solve the problems of less efficient process of chemical energy stored in a fuel, released as the heat of combustion is less efficient, etc., and achieves limited charge/discharge cycle life and avoid safety problems.
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first embodiment
[0057] A, the disclosure provides a method of forming a dried, water-solvated glass / amorphous solid. The method includes transforming a crystalline, sodium ion (Na+) or lithium-ion (Li+) electronic insulator or its constituent precursors comprising at least one Na+ or Li+ bonded to oxygen (O), hydroxide (OH), and / or to at least one halide into a water-solvated glass / amorphous Na+ or Li+ ion-conducting solid by adding water in an amount less than or equal to the water solvation limit of the glass / amorphous solid.
[0058]In further embodiments, which may be combined with embodiment A and with one another unless clearly mutually exclusive, i) the method further includes adding a glass-forming oxide, sulfide, or hydroxide and heating to expel volatile constituents; ii) the crystalline, electronic insulator or its constituent precursors include a material with the general formula A3-xHxOX, wherein 0≤x≤1, A is the at least one alkali metal, and X is the at least one halide; iii) the crystal...
second embodiment
[0059] B, the disclosure provides a method of forming an H+-conductive water-solvated electrolyte. The method includes transforming a crystalline material comprising at least one alkali and / or alkaline-earth cation bonded to at least one acidic polyanion into a glass / amorphous solid by adding water in an amount less than or equal to its solvation limit in the crystalline material such that water dissociates into hydroxide (OH)− anions that coordinate to the cations to form polyanions and the water also dissociates into protons (H+) that are mobile in a framework of an acidic oxide and the polyanions.
third embodiment
[0060] C, the disclosure provides a method of forming a water-solvated glass / amorphous solid. The method includes transforming a crystalline electronic insulator comprising at least one acidic polyanion and at least one cation into a water-solvated glass / amorphous proton (H+)-conducting solid by adding water in an amount less than or equal to the water solvation limit of the crystalline electronic insulator
[0061]In further embodiments, which may be combined with embodiments B or C, and with one another unless clearly mutually exclusive: i) wherein the acidic polyanion includes (SO4)2− and / or (PO4)3− and / or (SiO4)4− polyanion; ii) the at least one cation is stabilized in the form of at least one stable hydroxide polyanion; iii) the at least one cation includes a barium (Ba2+) ion, a potassium (K+) ion, a rubidium (Rb+) ion, and / or a cesium (Cs+) ion; iv) the stable hydroxide polyanion includes (Ba(OH)x)2-x, (K(OH)x)1-x, (Rb(OH)x)1-x and / or (Cs(OH)x)1-x.
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Abstract
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