The application discloses a kind of laboratory high-frequency induction
combustion after
tungsten combustion improver
recovery method, belong to
resource recovery technical field.The present application is to solve the carbon and
sulfur content of
tungsten particle that cannot meet the requirement of
trace analysis, provides a kind of laboratory high-frequency induction
combustion after
tungsten combustion improver
recovery method, comprising:A, crushing, acid
pickling, electromagnetic deironing complete pretreatment;B, alkali fusion
decomposition, convert tungsten into soluble
sodium tungstate;C, hot water leaching;D, two-stage purification
impurity removal;E, low-temperature acidification tungsten
precipitation, obtain high-purity
tungstic acid;F, high-purity
hydrogen reduction
roasting, obtain metallic tungsten;G, crushing and screening, obtain tungsten particle.The present application can obtain C<8ppm, S<5ppm qualified tungsten particle, tungsten
recovery rate is ≥98%, can directly replace new tungsten particle and use, application effect is stable, reproducibility is good, and does not affect detection precision and
equipment safety, greatly reduce detection consumable cost.