Process for preparing orienting-reinforced aluminum -based composite material

An aluminum matrix composite material and directional reinforcement technology, which is applied in the field of metal matrix composite material preparation, can solve the problems of easy deformation of prefabricated blocks, uneven microstructure, serious interface reaction, etc., and achieve fine structure, wide application range, and interface reaction. small effect

Inactive Publication Date: 2009-07-29
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this method is limited by the characteristics of the metal matrix composite material prepared by the liquid pressure infiltration method. During the squeeze casting process, the prefabricated block is prone to deformation, the surface roughness is large after casting infiltration, the microstructure is uneven, and the grain size is large and dense. Disadvantages such as serious interface reaction

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] This embodiment is a method for preparing a directionally reinforced aluminum matrix composite material. The steps and process conditions of the preparation method are as follows:

[0028] In this embodiment, the aluminum-based composite material matrix adopts aluminum alloy component powder, and its composition is: by mass percentage, Si powder with a particle size of 20 μm, 20% of Si powder, 3% of Cu powder with a particle size of 20 μm, and the rest with a particle size of 15 μm Al powder; the short fiber ceramic phase is Al 2 o 3 short fibre. Press Al 2 o 3 Short fiber: Al-20Si-3Cu aluminum alloy component powder = 1:6 mass ratio mixed to make aluminum matrix composite material powder, Al 2 o 3 Short fiber accounted for Al 2 o 3 10% of the total volume of short fibers and Al-20Si-3Cu aluminum alloy component powder. A polyvinyl alcohol solution with a mass concentration of 4% was prepared with polyvinyl alcohol with a degree of polymerization of 1750. Accor...

Embodiment 2

[0030] In this embodiment, Al powder is used as the matrix of the aluminum-based composite material, and the particle size is 60 μm. The short fibrous ceramic phases are SiC whiskers. According to SiC whisker: Al powder=63.6:216 mass ratio is mixed and made into aluminum matrix composite material powder, and SiC whisker accounts for 20% of the total volume of SiC whisker and Al powder. A polyvinyl alcohol solution with a mass concentration of 5% was formulated with polyvinyl alcohol with a degree of polymerization of 2000. According to the mass ratio of polyvinyl alcohol solution: aluminum-based composite material powder = 6.5: 100, add polyvinyl alcohol solution to the aluminum-based composite material powder, mix and stir evenly, and prepare aluminum-based composite material powder slurry. Then put the aluminum-based composite material powder slurry into a directional extrusion die for directional extrusion, the inner diameter of the nozzle of the directional extrusion die ...

Embodiment 3

[0032] In this embodiment, 2024 aluminum alloy powder with a particle size of 30 μm is used as the matrix of the aluminum-based composite material. The short fibrous ceramic phase is Si 3 N 4 whiskers. Press Si 3 N 4 Whiskers: 2024 aluminum alloy powder = 159:135 mass ratio mixed to form aluminum matrix composite material powder, Si 3 N 4 Whiskers occupy Si 3 N 4 50% of the total volume of whiskers and 2024 aluminum alloy powder. A polyvinyl alcohol solution with a mass concentration of 4.5% was formulated with polyvinyl alcohol with a degree of polymerization of 1870. According to the mass ratio of polyvinyl alcohol solution: aluminum-based composite material powder = 10:100, add polyvinyl alcohol solution to the aluminum-based composite material powder, mix and stir evenly, and prepare aluminum-based composite material powder slurry. Then put the aluminum matrix composite material powder slurry into a directional extrusion die for directional extrusion, the inner di...

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Abstract

The invention relates to a preparation method of directional reinforced aluminum matrix composite material. In this method, aluminum powder or aluminum alloy powder or aluminum alloy component powder, short fiber ceramic phase, and polyvinyl alcohol solution are evenly mixed to obtain a composite material powder slurry; then the composite material powder slurry is put into a directional extrusion mold Perform directional extrusion to prepare aluminum-matrix composite material green filaments with short-fibrous ceramic phase orientation reinforcement; after the filaments are dried and dried, stack the filaments along the length direction and press-form the aluminum-matrix composite material green body ; Finally, sintering the green body of the aluminum matrix composite material in a hydrogen or argon protective atmosphere furnace or a vacuum furnace to obtain a short fiber-shaped ceramic phase-oriented reinforced aluminum matrix composite material. The content range of the ceramic phase of the material is wide, the interface reaction with the aluminum alloy matrix is ​​small, and the degree of directional distribution is high, which is conducive to giving full play to the longitudinal performance advantages of the short fiber-shaped ceramic phase; in addition, the directional distribution process does not cause damage to the surface of the ceramic phase; preparation The device is simple and the operation is convenient.

Description

technical field [0001] The invention relates to the field of metal-matrix composite material preparation, in particular to a preparation method of directional reinforced aluminum-matrix composite material. Background technique [0002] As early as the 1980s, people have realized that the distribution of reinforcements such as whiskers or short fibers in the matrix of metal matrix composites, if the three-dimensional random state becomes a unidirectional arrangement, the reinforcement of whiskers or short fibers The effect will be greatly improved. At present, although the secondary processing of aluminum matrix composites (such as rolling, extrusion, etc.) can achieve the orientation and orderly arrangement of whiskers or short fibers in the vertical direction of force, this method whiskers or short fibers The degree of orientation is not high, and it is easy to cause damage to whiskers or short fibers. Based on this point, people began to try the method of directional dis...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F3/20
Inventor 陈维平尚俊玲李元元李小强肖志瑜
Owner SOUTH CHINA UNIV OF TECH
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