Compounding of inorganic anti-pollution coating for high pressure insulator surface and preparation process thereof
A technology of anti-fouling flashover coatings and high-voltage insulators, which is applied in the direction of art coatings, insulators, coatings, etc., to achieve high chemical stability, convenient operation, and avoid safety hazards and additional costs.
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[0014] The preparation method of formula 1: (1): Hydrolyze the titanium alkoxide under the condition of acidic pH7 to obtain a uniform and transparent sol, adjust the pH value of the sol to 1-5 by dialysis, Prepare pure titanium dioxide sol; (2): add hydrogen peroxide with a weight ratio of 0.01 to 1.0% into the pure titanium dioxide sol to prepare an inorganic antifouling flashover coating.
[0015] The preparation method of formula 2: (1): prepare the binary composite oxide sol of titanium dioxide, and adjust the pH value to 1-5; (2): add the binary composite oxide sol of titanium dioxide in a weight ratio of 0.01- 1.0% hydrogen peroxide to prepare an inorganic antifouling flashover coating.
[0016] Inorganic anti-pollution flashover coating is used for off-line coating on the surface of newly prepared conventional insulators. The off-line coating method is: first clean the surface of the insulator, and then spray the paint on the surface of the insulator after drying until...
Embodiment 1
[0020] Formulation 1: Preparation of inorganic antifouling flashover coating
[0021] Add 1.1mL of concentrated nitric acid (68%) into 150mL of deionized water to make a uniform solution, slowly drop 12.5mL of tetraisopropyl titanate into the acidic aqueous solution under vigorous stirring, and hydrolyze the obtained suspension containing white precipitate Stirring was continued at 40 °C until the white precipitate dissolved to form a homogeneous transparent sol. Put the sol into a dialysis membrane bag and use 1L deionized water for dialysis treatment, and change the water every 8 hours until the final pH value of the dialysis water is 3.2. The sol was taken out from the dialysis bag to prepare a titania sol with a weight content of about 2.5%.
[0022] Under vigorous stirring, 0.1 mL of hydrogen peroxide reagent was added to the prepared 100 mL of titanium dioxide sol, and the inorganic anti-fouling flashover coating A was obtained after stirring evenly.
Embodiment 2
[0024] Formula 2: Preparation of Inorganic Antifouling Flashover Coating
[0025] Under vigorous stirring, slowly drop 10 mL of tetraethyl orthosilicate into a solution prepared by 0.5 mL of concentrated nitric acid (68%) and 20 mL of deionized water, and continue stirring until a uniform transparent silica sol is formed. Stir and mix 10 mL of this sol with 100 mL of the titanium dioxide sol prepared in Example 1, and then perform the same dialysis treatment as in Example 1 to adjust the pH value to 2.8. In this sol, the weight content of titanium dioxide is 2.3%, the weight content of silicon dioxide is 1.1%, and the pH value is 2.8.
[0026] 0.1 mL of hydrogen peroxide reagent was added to the prepared 100 mL of titanium dioxide-based composite sol, and the inorganic antifouling flashover coating B was obtained after stirring evenly.
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