Method of preparing carbon-based high valence silver molecule crystal battery
A molecular crystal, high-valent silver technology, applied in the direction of sterilization/microdynamic water/sewage treatment, etc., can solve the problem of large grain size of carbon-based high-valent silver molecular crystal battery, achieve strong chemical adsorption capacity and chemical reactivity, Performance-enhancing effects
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Embodiment 1
[0016] (1) Weigh 0.5 grams of AgNO 3 , Dissolved in 1000 ml of pure water, and then placed 1000 g of activated carbon in a silver nitrate solution under stirring for 30 minutes to filter, filter out the water and detect the silver content in the water. The filtered activated carbon is dried at 105°C for later use;
[0017] (2) Weigh 48.0 grams of per(2) potassium sulfate in distilled water, and then add 48.0 grams of KOH. Then dilute to 1000 grams, heat to 85-90℃, react with dried activated carbon under tumbling and stirring, keep at 90℃ for 30 minutes, filter, and rinse with pure water four times to wash away potassium sulfate, potassium nitrate and others on the activated carbon Impurities, the carbon-based high-valent silver molecular crystal battery is obtained. Then every 1000g of activated carbon contains Ag 4 O 4 0.47g crystals.
[0018] 15g of the carbon-based high-valent silver molecular crystal battery prepared and activated according to Example 1 was put into a φ33mm gl...
Embodiment 2
[0020] (1) Weigh 1.0 g of silver nitrate and dissolve it in 1000 ml of pure water, then place 1000 g of activated carbon in the silver nitrate solution under stirring for 30 minutes to filter, filter out the water and detect the silver content in the water, and then filter the dried activated carbon Dry at 105℃ for use;
[0021] (2) Weigh 24-90 grams of oxidizing agent per (two) sodium sulfate in distilled water, add 48-60 grams of sodium hydroxide, and then dilute to 1000 grams, heat to 85-90℃, tumbling and stirring and drying Activated carbon reaction, keep at 90°C for 30 minutes, filter, and rinse with pure water four times to wash away sodium sulfate, sodium nitrate and other impurities on the activated carbon to obtain a carbon-based high-valent silver molecular crystal battery. Then every 1000g of activated carbon contains Ag 4 O 4 Crystal 0.94g.
[0022] 15g of the carbon-based high-valent silver molecular crystal battery prepared and activated according to Example 2 is put...
Embodiment 3
[0024] (1) Weigh 0.75 g of silver nitrate and dissolve it in 1000 ml of pure water, then place 1000 g of activated carbon in the silver nitrate solution under stirring for 30 minutes to filter, filter out the water and detect the silver content in the water, and then filter the dried activated carbon Dry at 105℃ for use;
[0025] (2) Weigh 24-90 grams of oxidizing agent per (two) potassium sulfate in distilled water, add 48-60 grams of potassium hydroxide, and then dilute to 1000 grams, heat to 85-90°C, tumbling and stirring and drying Activated carbon reaction, keep at 90°C for 30 minutes, filter, and rinse with pure water four times to wash away potassium sulfate, potassium nitrate and other impurities on the activated carbon to obtain a carbon-based high-valent silver molecular crystal battery. Then every 1000g of activated carbon contains Ag 4 O 4 Crystal 0.70g.
[0026] 15g of the carbon-based high-valent silver molecular crystal battery prepared and activated according to Ex...
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