Nano-stage ceramic metal additive for lubricating oil and preparation thereof
A ceramic-metal, nano-scale technology, applied in the direction of additives, lubricating compositions, petroleum industry, etc., can solve the problems of single unit performance, unsatisfactory use effect of pure metal base and pure ceramic base, etc.
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[0014] 1. Preparation of nanoparticle powder
[0015] Hydrolyze borate and deionized water in a high-speed stirring mixer mixer, add sodium nitride and hydrazine hydrate respectively after the borate is completely dissolved, slowly raise the temperature and continue stirring until completely dissolved; add coupling agent and ethanol, Heating; add ammonium molybdate when the solution is transparent; add copper sulfate after the solution is stable; Salt Alcohol Sol. The material components used are calculated based on the product components. The sol is pumped into the autoclave, and the air in the autoclave is exhausted with nitrogen. After the autoclave is sealed, it is heated slowly, and samples are taken regularly to observe the shrinkage and aging degree of the gel until the double salt nuclei gel is in the autoclave. Until the aging is formed; after the gel is qualified, it is pressed into the airgel hybrid generator with a high-pressure pump in time, pressed out from the...
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