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222 results about "Crystallographic defect" patented technology

Crystallographic defects are interruptions of regular patterns in crystalline solids. They are common because positions of atoms or molecules at repeating fixed distances determined by the unit cell parameters in crystals, which exhibit a periodic crystal structure, are usually imperfect.

Method and apparatus for atomic layer deposition of a fluoride layer, optical element and optical arrangement

A method of depositing at least one fluoride layer comprises: depositing the fluoride layer on a substrate by photoassisted atomic layer deposition, ALD, in a plurality of ALD cycles. The method comprises irradiating the fluoride layer with UV / VIS light at least in some of the plurality of ALD cycles, such as in all ALD cycles, to anneal at least one potential crystal defect in the fluoride layer. The methods can be performed using an apparatus for atomic layer deposition of at least one fluoride layer, thereby producing an optical element comprising a substrate coated with such a fluoride layer, which can be used in an optical arrangement comprising at least one such optical element.
Owner:CARL ZEISS SMT GMBH

Low-defect gallium oxide single crystal pulling growth equipment and method based on double-cavity atmosphere regulation and control

The invention relates to the technical field of semiconductor material growth, and aims to solve the technical problems that the service life of a heating element is shortened due to single atmosphere sharing, the quality is difficult to guarantee due to many crystal defects, the single crystal production cost is high, and the production efficiency is low in the prior art. The invention discloses a single crystal growth device which is characterized by comprising a furnace body, a first chamber, a second chamber, a heating assembly, a growth assembly, an atmosphere isolation and heat conduction assembly, an atmosphere management system and a central control system, the atmosphere isolation and heat conduction assembly is used for separating the furnace body into a first cavity and a second cavity which are isolated in an airtight mode, and efficient heat transfer is achieved. By the adoption of the scheme, atmosphere structure separation and combined crucible design can be achieved, high quality and high purity of crystals are guaranteed, meanwhile, the service life of a heating element is effectively prolonged, and the operation cost is remarkably reduced.
Owner:BEIJING GACHUANG SEMICONDUCTOR EQUIPMENT CO LTD

Method for regulating and controlling strength and plasticity of FeMnCrCo-series high-entropy alloy based on pre-introduction of multi-dimensional crystallography defects

The invention discloses a method for regulating and controlling the strength and plasticity of a FeMnCrCo-series high-entropy alloy based on pre-introduction of multi-dimensional crystallography defects, and relates to the technical field of high-entropy alloy materials. Cleaning in the vacuum induction furnace; performing vacuum melting; casting is conducted; carrying out homogenization treatment; forging treatment; carrying out six-pass hot rolling treatment; first-pass cold rolling treatment; first low-temperature annealing treatment; performing second-pass cold rolling treatment; carrying out secondary low-temperature annealing treatment; third-pass cold rolling treatment; and annealing treatment. Inter-pass annealing treatment is introduced into a cold rolling link of a traditional plate preparation process, and water-cooling quenching is assisted. According to the method, the multi-dimensional crystallographic defects generated in the cold rolling process are reserved in an initial microstructure of the alloy before a mechanical property test, the crystallographic defect type, density and spatial distribution in the initial microstructure of the alloy are regulated and controlled, a multi-dimensional defect strengthening mechanism is constructed, and good strength and plasticity matching of the alloy is achieved.
Owner:SHENYANG UNIVERSITY OF TECHNOLOGY

Method for detecting abnormity of gallium oxide single crystal grown by Bridgman method based on multi-mode perception

The invention discloses a Bridgman method growth gallium oxide single crystal abnormity detection method based on multi-mode perception, and relates to the technical field of single crystal preparation, and the method comprises the following steps: S1, collecting optical signals of a melt surface area in a Bridgman method growth gallium oxide single crystal process through a sensor array, synchronously acquiring temperature field data or infrared thermal image data of the region; the method comprises the following steps: acquiring an original spectral data set covering a local area according to a radiation signal under a micron-order spatial resolution, and obtaining initial radiation distribution information; according to the anomaly detection method for growing the gallium oxide single crystal by the Bridgman method based on multi-mode perception, dynamic tracking and accurate positioning of component anomaly in the growth process of the Bridgman method are realized, and an effective technical means is provided for improving the growth quality of the gallium oxide single crystal, reducing crystal defects and improving the process control capability.
Owner:SHANDONG SDIC HLDG GRP CO LTD

Calcium fluoride crystal defect detection system and method

The invention provides a calcium fluoride crystal defect detection system and method, and relates to the technical field of detection, and the method comprises the following steps: preprocessing a crystal to determine a reference position and environmental parameters, and then respectively carrying out optical uniformity detection and stress birefringence detection to obtain an interference fringe pattern and polarization state change data; and optical path difference data and stress field data are generated. And through spatial registration and data association analysis, extracting areas with both refractive index anomaly and stress anomaly as candidate defect areas, quantifying defect strength and stress influence range, and finally outputting a quality judgment result of the crystal defect. The method improves the defect detection precision and reliability, and is especially suitable for high-precision calcium fluoride crystal quality control.
Owner:HENAN MICRON OPTICAL TECH CO LTD

Method and system for real-time regulation and control of crystal orientation in micron-sized single crystal growth process

The invention belongs to the technical field of crystal growth, and relates to a method and a system for regulating and controlling the crystal orientation in real time in a micron-sized single crystal growth process, which are used for realizing real-time microscopic monitoring on the crystal growth state by collecting inherent physical signals of a crystal growth interface area and generating original signal data. Extracting characteristic parameters associated with crystal orientation deviation from the original signal data, generating a crystal orientation deviation characteristic vector, inputting the crystal orientation deviation characteristic vector into a preset mapping model, generating a crystal orientation deviation quantitative index to calculate a local thermal field regulation and control instruction, the micro heat source array is driven to apply a local thermal field gradient to a target area of a crystal growth interface so as to guide the crystal orientation to return, so that global thermal stress fluctuation and new crystal defect hidden dangers caused by traditional large-range thermal field adjustment are avoided, flexible fine adjustment of the crystal orientation is realized, the internal quality and uniformity of crystal growth are greatly improved, and the crystal growth efficiency is improved. Therefore, the single crystal quality and the yield are obviously improved.
Owner:ZHONGSHAN GUANGDA OPTICAL INSTR CO LTD

FPD test method for micro-viewpoint defect of monocrystalline silicon wafer

The invention belongs to the technical field of crystal defect testing, and particularly relates to an FPD testing method for a monocrystalline silicon wafer micro-viewpoint defect, which comprises the following steps: accurately cutting off the head and the tail of a silicon rod to eliminate an end defect, and preparing a pure substrate by adopting an A-surface machine grinding / B-surface maintaining asymmetric treatment and segmented cleaning process; after pretreatment with a specifically proportioned corrosive liquid, carrying out temperature-controlled etching by using potassium dichromate-hydrofluoric acid to form a characteristic V-shaped pattern on the surface, and realizing visual identification by corresponding different defects to different patterns; gridding detection points are designed based on stress distribution, laser positioning coordinate mapping is performed, an imaging-correction-noise reduction-segmentation-intelligent classification algorithm chain is constructed to realize full-automatic detection, and a detection-analysis-optimization full-process data driving quality control system is established through visual data such as a thermodynamic diagram and a type matrix. And large-scale production of semiconductor silicon wafers is supported.
Owner:BEIJING MAIZHUJI TECH CO LTD

Preparation method of controlled-release magnesium hydroxide fertilizer

The invention relates to the technical field of inorganic material synthesis, in particular to a preparation method of a controlled-release magnesium hydroxide fertilizer. Comprising the steps of primary magnesium precipitation, hydrothermal treatment, secondary magnesium precipitation, anaerobic heat treatment and pulping. According to the method, firstly, crystal defects are eliminated through hydro-thermal treatment, crystal seeds with complete crystallinity are obtained, then the crystal seeds are added into a magnesium precipitation reaction system, the principle of Gibbs free energy minimization is followed, newly generated magnesium hydroxide tends to precipitate on the surfaces of the crystal seeds, under the interference effect of a crystal form regulator, the newly generated magnesium hydroxide crystal has many defects, and the magnesium precipitation effect is good. And then oxygen-free heat treatment is carried out, so that the defects of the magnesium hydroxide on the surface layer are further increased, and the initial dissolution and release capacity is improved. The controlled-release magnesium fertilizer which is high in early-stage release speed and long-acting in later-stage slow release is synthesized by utilizing a crystal defect engineering tool, and is different from a traditional coating scheme, and a brand new thought is provided for the design of the controlled-release fertilizer.
Owner:DALIAN MARITIME UNIVERSITY

A method for rapid non-destructive testing of silicon carbide crystal quality

The application discloses a method for rapidly and nondestructively detecting the quality of silicon carbide crystals, which comprises the following steps: placing the silicon carbide crystals on a computer tomography (CT) carrier table, and rapidly and nondestructively detecting the typical defects in the silicon carbide crystals by means of computer tomography under specific parameters, image contrast and the identification of the topographic features, so as to directly obtain the defect topography, density distribution and the evolution of the defects with the growth process of the measured ingot at different sections, and significantly improve the visualization degree of the defects in the silicon carbide crystals.
Owner:XIAMEN UNIV

Silicon carbide crystal growth method and device and silicon carbide crystal

The embodiment of the invention provides a silicon carbide crystal growth method and device and a silicon carbide crystal, relates to the technical field of silicon carbide crystal growth, and aims at solving the technical problem that in the prior art, due to the fact that gas phase flow cannot be dynamically adjusted, crystal defects are easily caused. The method comprises the steps that S1, seed crystals and silicon carbide powder are arranged in a crucible, and the crucible is connected with a gas phase flow adjusting assembly; s2, pumping air from the crucible, filling inert gas into the crucible, and heating the crucible to enable the silicon carbide crystals to enter a growth stage; and S3, in a crystal growth stage, controlling the opening degree of a gas-phase flow channel through a gas-phase flow adjusting assembly so as to adjust the flow of gas reaching the seed crystal until the growth of the silicon carbide crystal is finished. The method can effectively improve the crystal growth rate in the early and middle stages of crystal growth and avoid the carbon wrapping defect of the crystal in the later stage of crystal growth.
Owner:TONGWEI MICROELECTRONICS CO LTD

Method for detecting epitaxial growth temperature

The invention relates to an epitaxial growth temperature detection method, which comprises the following steps: providing a test wafer which comprises a calibration wafer and a temperature measurement wafer; performing defect treatment on the calibration wafer and the temperature measurement wafer so as to introduce crystal defects into the calibration wafer and the temperature measurement wafer; performing defect repair treatment on the calibration wafer at different target calibration temperatures, and obtaining defect repair information at corresponding temperatures; according to the target calibration temperature and the corresponding defect repair information, establishing a temperature measurement database used for representing the corresponding relation between the crystal state and the growth temperature; transferring the temperature measurement wafer into epitaxial equipment, and raising the temperature of the epitaxial equipment to an epitaxial temperature; obtaining crystal state information of the temperature measurement wafer at different positions; and obtaining the growth temperature corresponding to each crystal state based on the temperature measurement database and the crystal state information of the temperature measurement wafer. According to the epitaxial growth temperature detection method, temperature distribution in the epitaxial process can be effectively monitored and optimized, and the quality of a silicon carbide epitaxial film and the performance stability of a device are remarkably improved.
Owner:BEIJING SMART ENERGY RES INST +1

Wide-temperature-range perovskite optical storage material and preparation method and application thereof

The invention discloses a wide-temperature-range perovskite optical storage material and a preparation method and application thereof, the chemical general formula of the wide-temperature-range perovskite optical storage material is CsCdCl3: xSb < 3 + >, yMn < + >, Mn < + > is Zr < 4 + >, Sn < 2 + >, Hf < 4 + > or Gd < 3 + >, x is more than 0 and less than 0.06, and y is more than 0 and less than 0.02. The perovskite crystal can generate free carriers under excitation of X-rays or 365-nanometer ultraviolet light, the carriers can be stored in a crystal defect trap, and the storage temperature of the carriers covers an ultra-wide temperature range from 100 K to 350 K, so that wide-temperature-range X-ray imaging, information storage and anti-counterfeiting application can be realized.
Owner:HUAQIAO UNIVERSITY

Barium titanate spherical powder production method

The invention relates to the technical field of barium titanate production and preparation, in particular to a barium titanate spherical powder production method. The preparation method comprises the following steps: preparing and atomizing a precursor solution, then spraying the atomized precursor solution into a high-temperature reaction furnace for flame melt crystallization, and then carrying out gradient cooling and spherical curing in a cooling area of the high-temperature reaction furnace, and finally, grading and collecting the prepared spherical barium titanate powder through a collecting system to obtain spherical barium titanate powder with uniform particle size, and carrying out surface functionalization treatment on the collected spherical barium titanate powder through a coating unit to obtain surface-coated spherical barium titanate powder. The precursor solution is subjected to solvent evaporation, thermal decomposition and flame melting in a high-temperature reaction furnace to form barium titanate crystal nucleuses, the crystal nucleuses naturally shrink to form balls under the driving of surface tension, the defect of mechanical damage of a traditional solid phase method or the defect of agglomeration of a liquid phase method is overcome, the crystal defects of the crystal nucleuses are reduced, and meanwhile particle size distribution is more uniform.
Owner:JACQUESHENKO (CHENGDU) ELECTRONIC MATERIALS CO LTD

Thermal barrier coating (TBC) material with high fracture toughness, calcia-magnesia-alumino silicate (CMAS) corrosion resistance, and ultra-high-temperature sintering resistance, and preparation and use thereof, and tbc

A thermal barrier coating (TBC) material with high fracture toughness, calcia-magnesia-alumino silicate (CMAS) corrosion resistance, and ultra-high-temperature sintering resistance, and a preparation and use thereof are provided, belonging to the technical field of high-temperature / ultra-high-temperature TBCs. In the TBC material, ZrO2 is co-doped with different rare earth oxides and a crystal defect concentration and a lattice distortion degree are controlled by a doping amount of the rare earth oxides, resulting in a fully-stabilized cubic fluorite crystal structure showing no phase change at a room temperature to 1,600° C. Moreover, the material exhibits high toughness, CMAS corrosion resistance, ultra-high-temperature sintering resistance, and long service life.
Owner:EAST CHINA UNIV OF SCI & TECH +2

7N single crystal copper preparation process based on zone melting and crystal orientation control

The invention discloses a 7N single crystal copper preparation process based on zone melting and crystal orientation control, which specifically comprises the following steps: S1, raw material pretreatment: purifying 4N copper to 5N grade by adopting electrolytic refining of a nitric acid system, and the carbon content after acid pickling is less than or equal to 1ppm; the invention relates to the technical field of metal material preparation. According to the 7N single crystal copper preparation process based on zone melting and crystal orientation control, impurities in a material are redistributed in a melting zone through local heating, so that separation and removal of the impurities are achieved, in single crystal copper preparation, zone melting can remarkably reduce the content of the impurities in copper, the purity of the copper is improved, and the yield of the 7N single crystal copper is improved. By accurately controlling parameters such as the temperature gradient and the cooling rate in the smelting and solidification process, optimization of crystal orientation is achieved, single crystal copper with an ideal crystal structure can be obtained, the performance of the single crystal copper is improved, and impurities can be removed and crystal defects can be reduced through zone smelting; and crystal orientation control can optimize the crystal structure and improve the performance.
Owner:JIANGSU XINRUILONG NEW MATERIAL TECH CO LTD

Crystal growth temperature control method and related device

The invention discloses a temperature control method for crystal growth and a related device, and the method comprises the steps: firstly obtaining image data in a crystal growth process, then extracting an aperture image from the image data, obtaining a plurality of aperture thicknesses corresponding to a plurality of positions in the aperture image according to a fixed angle, and carrying out the temperature control of the crystal growth, and then the temperature is controlled based on the ratio of the number of the aperture thicknesses exceeding the preset threshold to the total number of the apertures corresponding to the plurality of aperture thicknesses, so that whether the number of the aperture thicknesses exceeding the preset threshold is too large or too small can be determined by analyzing the image of the aperture part on the surface of the crystal; whether the single crystal grows uniformly or not and whether the temperature is appropriate or not are judged and determined, the cost is low, the anti-interference capacity is high, accurate temperature information can be obtained, the crystal can grow uniformly by controlling the temperature in the crystal growth process, crystal defects are avoided, and the crystal quality is improved.
Owner:BAODING JING XIN SHI CHUANG ELECTRIC

Method for growing large-size CLBO crystal by using new fluxing agent

The invention discloses a method for growing a large-size CLBO crystal by using a new fluxing agent, and belongs to the field of nonlinear optical crystals. The adopted new fluxing agent is Cs2O-Li2O-B2O3-YF3, and the large-size CLBO crystal can be obtained through growth by a high-temperature solution top oriented seed crystal growth method. According to the novel fluxing agent, the solution viscosity can be effectively reduced, and crystal defects are reduced; and the grown large-size CLBO crystal has the advantages of high transmittance, strong deliquescence resistance and the like, and can be used as a frequency doubling device of an ultraviolet laser.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY

High-precision laser etching method for high-thermal-conductivity metal film on surface of organic material

The invention relates to a novel high-precision laser etching method for a high-thermal-conductivity metal film on the surface of an organic material. According to the principle that the arrangement mode of atoms in crystal lattices is determined by crystal defects, crystal sizes and crystal orientations in metal materials, so that the transfer mode of heat energy through phonons and electrons is influenced, and by regulating and controlling the crystal structures of the metal materials, the transverse heat conduction area of instantaneous laser energy in the metal film is reduced; therefore, the energy longitudinally conducted to the interface of the metal film and the substrate under the action of the laser is increased, so that the temperature of the interface of the laser spot edge area is higher than the thermal decomposition temperature of the substrate material, and the solid stripping phenomenon is generated. The method provided by the invention solves the problem that high-thermal-conductivity metal subjected to laser etching is easy to remain at present, improves the precision of a laser etching pattern, and has scientific and industrial practical potential.
Owner:LANZHOU INST OF PHYSICS CHINESE ACADEMY OF SPACE TECH

Surface etching method for exposing dislocation defect of tellurium indium lead single crystal

The invention discloses a surface etching method for revealing dislocation defects of tellurium indium lead single crystals, and relates to a method for revealing crystal defects. The invention aims to provide a surface etching method capable of accurately exposing crystal defects. The method comprises the following steps: firstly, carrying out directional cutting, multi-stage mechanical polishing and chemical mechanical polishing on a PIT single crystal to obtain a smooth and damage-free surface; and reacting iodine with concentrated nitric acid to generate iodic acid as a main oxidant, adding hydrofluoric acid for activation, diluting with an acetic acid-water mixed solution, and etching the crystal at a low temperature of 10 + / -1 DEG C under ultrasonic assistance. According to the method, the regular triangular conical etching pit can be formed on the PIT single crystal (001) surface, the depth is 100-300 nm, the pit bottom points to the [001] direction, and the dislocation defect is clearly revealed. The method has the advantages of clear etching morphology, high sensitivity, high reliability and simplicity and convenience in operation, and can be applied to the fields of PIT single crystal quality evaluation, defect analysis and growth process optimization.
Owner:HARBIN INST OF TECH

Thickness-controllable SSZ-13 molecular sieve separation membrane as well as preparation method and application thereof

The invention discloses a thickness-controllable SSZ-13 molecular sieve separation membrane and a preparation method and application thereof.The SSZ-13 molecular sieve separation membrane comprises a seed crystal layer, the seed crystal layer is formed in the mode that SSZ-13 molecular sieve crystals are subjected to ball milling treatment to form nanoscale particles, the nanoscale particles are loaded on the outer surface of a hollow fiber carrier through a dip-coating technology, and the SSZ-13 molecular sieve separation membrane is prepared. The thickness of the seed crystal layer is the same as that of the SSZ-13 molecular sieve membrane. A ball-milled seed crystal layer with crystal defects and a zeolite precursor nano-cluster in gel are assembled and healed in a short time to form a continuous defect-free film layer, and the thickness of the seed crystal layer is changed by adjusting the dipping and coating time and the concentration of a seed crystal liquid, so that the thickness of a corresponding film is changed, and the film is prepared. The prepared SSZ-13 molecular sieve membrane shows ultrahigh CO2 permeability and CO2 / CH4 selectivity; the H2S-resistant stability is extremely high, the repeatability is high, and the large-scale production of the molecular sieve membrane for gas separation is facilitated.
Owner:NANJING TECH UNIV

Method for improving room-temperature gas-sensitive performance of metal oxide semiconductor sensitive material

The invention discloses a method for improving the room-temperature gas-sensitive property of a metal oxide semiconductor sensitive material, which comprises the following steps of: uniformly placing the metal oxide semiconductor sensitive material on a pressing plate of a rotary shearing machine, and then applying pressure to the metal oxide semiconductor sensitive material until the target pressure is reached; and then directly standing or standing after high-pressure torsion, and finally relieving the pressure to obtain the metal oxide semiconductor sensitive material after high-pressure treatment or high-pressure shearing treatment. The high-pressure torsion is to rotate a side chopping board and apply different shear revolutions to the metal oxide semiconductor sensitive material. The sensitive material rich in crystal defects and bulk strain is successfully prepared through a high-pressure technology or a high-pressure torsion technology, more active sites are provided for gas molecule adsorption and reaction, crystal field distortion is induced to change the electronic structure of the material, and therefore the response performance of the sensitive material to specific gas is improved, and the sensitivity of the sensitive material to the specific gas is improved. And the gas-sensitive material has excellent gas-sensitive selectivity in various gas tests.
Owner:NORTHEAST NORMAL UNIVERSITY

A method for preparing high-performance platinum micro-wire

The application relates to a preparation method of high-performance platinum fine wires and belongs to the field of metal materials. By adopting high-frequency vibration casting, the method can extrude gas and impurities in fluid liquid crystals, reduce crystal defects in the metal grain crystallization process, improve the material density, and improve the comprehensive mechanical properties of the material. The application solves the problems of high wire breakage rate, poor uniformity and stability of pure platinum fine wires. The product is especially suitable for rapid wire pairing of pure platinum with a wire diameter of Phi 0.01mm-Phi 0.02mm and platinum resistance wires.
Owner:ITP CO LTD(CN)

Crystal position adjusting mechanism of crystal defect detection device

The utility model discloses a crystal position adjusting mechanism of a crystal defect detection device, which comprises a cabinet body, a cabinet door is arranged on the cabinet body, detection components are arranged on the cabinet body and the cabinet door, and a displacement component is arranged in the cabinet body. According to the utility model, after the crystal is clamped, the two L-shaped plates drive the crystal to move towards the center of the cabinet body, and because the balls are higher than the supporting base and the bottom of the crystal is higher than the supporting base, the crystal is not contacted with the supporting base during movement, and when the extension lengths of the two electric telescopic rods are consistent, the crystal is located at the center of the cabinet body; at the moment, the electric telescopic rods are stopped, the two electric telescopic rods are retracted, the crystal falls to the center position of the supporting base, and due to the fact that the crystal is moved through the two electric telescopic rods at the moment, the crystal cannot be pushed in one direction, the crystal can move forwards or deviate due to inertia when the electric telescopic rods stop moving, and it can be guaranteed that the crystal is in a straightening state and is centered.
Owner:SHENZHEN UNIV

Hollow core fiber and optical communication systems

To provide a photonic bandgap type vacant core fiber suitable for transmission in two wavelength bands, and an optical communication system using the same. [Solution] The porous core fiber comprises a cladding portion having a porous structure arranged to surround the porous core portion and form a photonic crystal in which the porous core portion is a crystal defect, and propagates a first light having a wavelength of 1000 nm to 1150 nm and a second light having a wavelength of 1530 nm to 1625 nm in the porous core portion, and the transmission loss of the first light is 10 times or less the transmission loss of the second light.
Owner:FURUKAWA ELECTRIC CO LTD

Flexible flow guide ring, preparation method and silicon carbide crystal growth method applying flexible flow guide ring

The invention relates to the technical field of semiconductor materials, and particularly discloses a flexible flow guide ring, a preparation method and a silicon carbide crystal growth method applying the flexible flow guide ring. The flexible flow guide ring comprises any one or more of tantalum carbide, tungsten carbide, molybdenum carbide, niobium carbide and zirconium carbide. The preparation method of the flexible flow guide ring comprises the following steps: placing a flexible flow guide ring blank in heat treatment equipment containing silicon carbide powder or carbon powder, vacuumizing, filling argon, carbonizing, and obtaining the flexible flow guide ring after carbonization is finished. The silicon carbide crystal growth method using the flexible flow guide ring comprises the following steps: assembling the flexible flow guide ring and a crucible containing silicon carbide seed crystals and silicon carbide powder, transferring the crucible to a single crystal growth furnace after the assembly is completed, growing the silicon carbide crystals by using a PVT method, and obtaining the high-quality silicon carbide crystals after the growth is completed. The problems of crystal defects and flow guide ring cracking in the growth process of the silicon carbide crystal can be reduced.
Owner:JIANGSU CHAOXINXING SEMICON CO LTD

Samarium-iron-nitrogen magnetic powder and preparation method and application thereof

The invention provides samarium-iron-nitrogen magnetic powder and a preparation method and application thereof, the samarium-iron-nitrogen magnetic powder comprises a first samarium-iron-nitrogen particle, the surface of the first samarium-iron-nitrogen particle is provided with at least one step structure, and each step structure comprises at least two layers of steps. The surface of the first samarium-iron-nitrogen particle is of a step structure, the first samarium-iron-nitrogen particle is high in density, few in crystal defect and high in intrinsic coercive force, and when the samarium-iron-nitrogen magnetic powder comprising the first samarium-iron-nitrogen particle is applied to preparation of a magnet, the residual magnetism and the intrinsic coercive force of the magnet can be improved, and the service life of the magnet can be prolonged.
Owner:JINLONG RARE EARTH INNOVATION TECHNOLOGY (XIAMEN) CO LTD +1

Substrates for optoelectronic devices and methods of manufacturing same

There is described a method of manufacturing a substrate for an optoelectronic device. The method has the steps of: supporting a first layer of a first crystalline material on a second layer of a second crystalline material different from said first crystalline material thereby exposing crystalline defects at a surface of said first layer; etching said first layer using first etching conditions, at least some of said crystalline defects expanding into pores running from said surface of the first layer towards said second layer; and heating said first and second layers up to a first temperature for a first period of time within a given environment, said heating transforming said pores into nanovoids attracting at least some of said crystalline defects away from said surface. In some embodiments, the method has a step of reheating the layers or a step of forming a pore containing region within the first layer.
Owner:SCOPRA SCI & GENIE SEC

Quantum transistor

A quantum computing device includes an optical resonator having a resonant wavelength band. A crystalline material including a crystal defect is contained within the optical resonator. The crystal defect has a ground state and an excited state, which has an emission wavelength in the resonant wavelength band. A source electrode and a drain electrode are disposed on opposing sides of the crystal defect and configured to apply a first electric field in the crystalline material along a longitudinal axis. A gate electrode is disposed in proximity to the crystal defect and configured to apply to the crystalline material a second electric field transverse to the longitudinal axis. Control circuitry is configured to apply a first voltage between the source and drain electrodes to control a charge state of the crystal defect and to apply a second voltage to the gate electrode to tune the emission wavelength.
Owner:QUANTUM TRANSISTORS TECH LTD

Micro-scale analysis method for structural composition of oxide on surface of reinforcing steel bar

The invention relates to the technical field of material analysis, and discloses a reinforcing steel bar surface oxide structure composition microscale analysis method, which comprises the following steps: obtaining a high-fidelity sample through a layered inert protection sample preparation technology, and sequentially analyzing oxide microstructure and element distribution by adopting a scanning electron microscope-energy spectrum coupling technology, atomic-scale crystal defect observation is realized by combining a spherical aberration correction transmission electron microscope, macroscopic phase composition and microcell chemical valence information are respectively acquired synchronously through X-ray diffraction and X-ray photoelectron spectroscopy, and finally a cross-scale correlation model covering morphological characteristics, crystal structures, phase distribution and chemical states is constructed through multi-source data fusion. And micro-scale structure analysis is realized. Through combination of a multi-source characterization technology, steel bar oxide cross-scale analysis is realized, a high-fidelity sample preparation technology is adopted to guarantee an original state of a sample, a chloride ion diffusion quantitative model fused with crystal defect parameters is constructed, and rust layer protection evaluation is improved from qualitative observation to quantitative prediction.
Owner:HENAN ACADEMY OF SCI CHEM RES INST CO LTD

A method for improving the performance of a perovskite cell by grain boundary passivation

The application belongs to the method for improving the energy conversion efficiency and stability of organic-inorganic hybrid perovskite solar cells, and the main content is that ethyl benzene sulfonyl lactam (PSAD) containing sulfonamide functional group is combined with-NH2 and Pb 2+ in perovskite material respectively through hydrogen bond and coordination effect to passivate the crystal defects caused by the two kinds of functional groups and cations in perovskite crystal grains. The oxygen atom of the sulfoxide group in PSAD can not only fix the organic amine ion in perovskite through hydrogen bond, but also can form Pb 2+ …O coordination bond with Pb to passivate the defects caused by Pb. The method passivates the grain boundary, reduces the non-radiation recombination of carriers, enhances the charge transport of perovskite thin film, and significantly improves the energy conversion efficiency and stability of perovskite solar cells. The additive PSAD is cheap and easy to obtain, which provides the possibility for industrialization.
Owner:QINGDAO UNIV OF SCI & TECH