Unlock instant, AI-driven research and patent intelligence for your innovation.

Porous ceramics Screen plate resisting low concentration hydrofluoric acid and preparation method thereof

A technology of porous ceramics and ceramic filter membranes, which is applied in the field of manufacturing low-concentration hydrofluoric acid-resistant porous ceramic filter plates. It can solve the problems of corroding ceramic filter plates, affecting the widening of the use range, and destroying filter plates, so as to improve the mechanical strength. Effect

Inactive Publication Date: 2010-05-19
江苏省陶瓷研究所有限公司
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Yet, all adopt clay and quartz etc. as binder (as Chinese patent CN01114048.8) in the formula of existing ceramic filter plate, its main component is SiO 2 Therefore, if hydrofluoric acid is used in chemical cleaning, it will corrode the ceramic filter plate, make it loose and lose its strength, causing the overall damage of the filter plate and accidents
At the same time, the adaptability of the ceramic filter plate to different materials, especially the adaptability to a small amount of hydrofluoric acid (<0.2g / l) in the pulp, affects the expansion of the scope of use of this type of ceramic filter
[0004] The improved microporous ceramic filter plate disclosed in Chinese patent 200510038128 and its preparation are all composed of titanium dioxide micropowder, which can only resist the corrosion of microfluorine (10-20mg / l), and will be limited for pulp with a fluorine content greater than 20mg / l

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] 1. According to the substrate formula ingredients in the following table

[0034] Material

[0035] Then add about 0.2 parts of dextrin and about 1.8 parts of water, and after fully mixing, press and form a single piece of filter. After drying, the green body is bonded into a filter plate substrate with a hollow structure. ℃ firing, machining to the required size.

[0036] 2. Use the ceramic membrane formula listed in the following table

[0037] Material

[0038] Then add about 0.4 parts of methyl cellulose and about 32 parts of water, mix and mill in a ball mill for 6-8 hours, and then evenly coat a 0.1-0.4mm thick ceramic film on the substrate, dry it below 100°C and dry it at 1200 ℃-1500 ℃ firing, sealing and assembling to get the finished product.

Embodiment 2

[0040] According to the following table ceramic filter plate formula ingredients

[0041] Material

Fused corundum

Nano alumina

Titanium dioxide

barium carbonate

magnesium fluoride

content%

60

10

15

10

5

[0042] Add about 0.15 parts of PVA, about 2.5 parts of water.

[0043] Use the ceramic membrane formula listed in the table below

[0044] Material

Fused corundum

γ-alumina

Nano alumina

Titanium dioxide

barium carbonate

magnesium fluoride

content%

62

5

13

8

4

8

[0045] Add about 0.25 parts of methylcellulose and about 30 parts of water.

[0046] Refer to Example 1 for the manufacturing method.

Embodiment 3

[0048] According to the following table ceramic filter plate formula ingredients

[0049] Material

Fused corundum

Nano alumina

Titanium dioxide

magnesium fluoride

content%

70

7

13

10

[0050] Add about 0.3 parts of dextrin and about 3.5 parts of water.

[0051] Use the ceramic membrane formula listed in the table below

[0052] Material

Fused corundum

Nano alumina

Titanium dioxide

barium carbonate

magnesium fluoride

content%

60

10

15

10

5

[0053] Add about 0.3 parts of methylcellulose and about 25 parts of water.

[0054] Refer to Example 1 for the manufacturing method.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
pore sizeaaaaaaaaaa
strengthaaaaaaaaaa
porosityaaaaaaaaaa
Login to View More

Abstract

The invention discloses a porous ceramic filtering plate with low-concentration hydrofluoric acid resistant, relating to a porous ceramic filtering plate used for solid-liquid separation of ore pulp of mineral oil industry. The invention consists of a base plate and the ceramic filtering film coated on the base plate; the base plate is compatible with organic binder; the ceramic filtering film isformed by the compatibility of capacitance corundum, alumina powder, mineralizer of non-silicon ceramic material, non-silicon pore-forming agent with organic binder, so as to produce the filtering plate which has not only ideal porosity rate (30-50 percent), suitable micropore size (2Mum or so) and good pressure (30-50MPa), but also has the performance of resistance of low-concentration hydrofluoric acid (with the concentration less than 0.2g / l) and working medium with pH value of 8-14; the invention can be washed by hydrofluoric acid and alkali and dehydrated and filter by ore pump containinga small quantity of hydrofluoric acid (less than 0.2g / l).

Description

technical field [0001] The invention relates to a porous ceramic filter plate used for solid-liquid separation of ore pulp in the mining industry, in particular to a ceramic filter plate that can be used for dehydration and filtration of ore pulp containing a small amount of hydrofluoric acid (<0.2g / l). It can also be cleaned with hydrofluoric acid, and at the same time it provides a manufacturing method of the low-concentration hydrofluoric acid-resistant porous ceramic filter plate. Background technique [0002] As a filter medium, the micropores of the ceramic filter plate of the ceramic filter will be blocked during use. In order to prevent the filter capacity from weakening, periodic chemical cleaning and ultrasonic cleaning are required. There are many kinds of substances that cause the clogging of ceramic filter plates, and the right medicine should be prescribed for chemical cleaning. The most common blockage in actual production is silica colloid, which cannot b...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): B01D39/20C04B35/10C04B38/00
Inventor 罗益军蒋建平邱永斌
Owner 江苏省陶瓷研究所有限公司