Method for producing slow digestion starch by hot-press acid-hydrolysis of cornstarch using organic acid

A technology of corn starch and digested starch, applied in the fields of application, food preparation, food science, etc., can solve the problems of unsuitable large-scale industrial production, high production cost, high cost, etc.

Inactive Publication Date: 2009-02-11
胡耀辉
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The physical method mainly uses microwave heating to treat starch, but this method is not suitable for large-scale industrial production and requires high production costs; enzymatic methods generally use pullulanase, isoamylase, etc. to enzymatically hydrolyze gelatinized starch , to obtain SDS through molecular modification technology, but the enzymes used in this method are high-cost enzymes, especially isoamylase, which are currently only used for laboratory sample preparation, and it will take a certain amount of time to be put into industrial production; according to literature reports The chemical reagents selected by the chemical method are toxic substances such as phosphorus oxychloride, octenyl succinic acid, and propylene oxide. Although the process is relatively simple, the prepared SDS has certain toxicity and cannot be applied to the field of food processing; However, the combination of physical and enzymatic methods to prepare SDS requires higher production costs than individual enzymatic methods, so it is unrealistic for industrial production.
On the other hand, the raw materials for the preparation of SDS are basically waxy corn starch, but the source of this raw material is not extensive.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Example 1: Slowly digestible starch produced by citric acid autoclaving and acid hydrolysis of common corn starch

[0034] Prepare 20L of citric acid aqueous solution with a concentration of 1.6% (w / v), weigh 2kg of ordinary cornstarch, mix the two to form cornstarch milk, stir mechanically for 30min to disperse the starch evenly, put the starch milk into the preheated autoclave The pot and the sealed pot cover start to heat up. When the temperature of the autoclave rises to 120°C, start timing for 15 minutes. During the whole process, the autoclave acidolysis temperature is controlled at 120±0.5°C. The starch milk that has been autoclaved and acid-hydrolyzed is subjected to centrifugation, the specific conditions are 4000rpm, 5min, centrifuged and washed 5 times, and the sediment is collected. After the sediment is sealed and packaged, it is placed in a refrigerator at 0°C for refrigerated regeneration for 24 hours. After the regeneration is completed, Remove the seale...

Embodiment 2

[0035] Embodiment 2: Slowly digestible starch produced by acetic acid pressing and heat acid hydrolysis of common corn starch

[0036] Prepare 30L concentration of 3% (w / v) acetic acid aqueous solution, weigh 3kg of common cornstarch, mix the two to form starch milk, mechanically stir for 30min to make the starch disperse evenly, put the starch milk into a preheated autoclave, Seal the pot lid and start to heat up. When the temperature of the autoclave rises to 110°C, start timing for 15 minutes. During the whole process, the autoclave acidolysis temperature is controlled to be 110±0.5°C. Use 1M NaOH to adjust the pH of the autoclaved and acid-hydrolyzed starch milk to 6.5-7.0, and then centrifuge it at 4000 rpm for 5 minutes. After centrifuging and washing for 4 times, the sediment is collected, and the sediment is sealed and packaged and placed in a Refrigerate and regenerate in a refrigerator at 0°C for 24 hours. After the regeneration is complete, remove the sealed package...

Embodiment 3

[0037] Example 3: Production of slowly digestible starch by malic acid pressing and heat acid hydrolysis of common corn starch

[0038] Prepare 20L of malic acid aqueous solution with a concentration of 1.4% (w / v), weigh 2kg of ordinary cornstarch, mix the two to form starch milk, stir mechanically for 30min to disperse the starch evenly, put the starch milk into a preheated autoclave , seal the pot cover and start to heat up, when the temperature of the autoclave rises to 120°C, start timing for 20 minutes, and control the autoclave acidolysis temperature to 120±0.5°C during the whole process. The starch milk that has been autoclaved and acid-hydrolyzed is subjected to centrifugation, the specific conditions are 4000rpm, 5min, centrifuged and washed 5 times, and the sediment is collected. After the sediment is sealed and packaged, it is placed in a refrigerator at 0°C for refrigerated regeneration for 24 hours. After the regeneration is completed, Remove the sealed package, put...

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PUM

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Abstract

The invention relates to a method for adopting organic acid to treat common corn starch through autoclaving and acid hydrolysis so as to prepare the slow digestible starch. The method includes the following steps: the common corn starch is prepared with the organic acid of 0.1 to 10 percent (w / v) concentration into a corn starch cream of 2 to 30 percent (w / v) concentration; the obtained corn starch cream is stirred for 20 to 60 minutes and then is treated through acid hydrolysis and autoclaving for 5 to 90 minutes under the temperature of 100 to 150 DEG C; then the corn starch cream is centrifuged at a speed of 2000 to 10000rpm for 2 to 10 minutes; the sediment of centrifugation is frozen for retrogradation under the temperature of minus 10 to 10 DEG C for 12 to 240 hours and then the sediment is dried with blast under the temperature of 50 to 80 DEG C for 10 to 20 hours; and then after the mechanical smashing, the sediment is sifted with a mesh sieve of 80 to 150 meshes so as to obtain the product containing more than 20 percent of slow digestible starch. The slow digestible starch prepared by the invention can be applied to the food manufacturing industry.

Description

technical field [0001] The invention belongs to the field of modified starch processing, and in particular relates to a method for producing slowly digestible starch by using organic acid, pressurization, and heat to acidolyze common corn starch. Background technique [0002] Starch is a very important food source of energy. Englyst divides starch into three categories according to its bioavailability, including Rapidly Digestible Starch (RDS), which can be digested by α-amylase in the small intestine within 20 minutes. Starch; slowly digestible starch (Slowly Digestible Starch, SDS), starch that can be digested by α-amylase in the small intestine within 20 to 120 minutes; resistant starch (Resistant Starch, RS), which cannot be digested by α-amylase in the small intestine after 120 minutes Digested starch. [0003] SDS has a variety of physiological functions: ①SDS stays in the gastrointestinal tract for a long time, releases glucose slowly, and the glucose produced can re...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/09A23L1/29A23L1/308A23L29/219A23L33/21
Inventor 胡耀辉王玉华于寒松刘俊梅戴建立李彩霞
Owner 胡耀辉
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