Copper plating bath for coating copper and method for surface copper plating permanent magnetic material using the same
A permanent magnet material, copper plating solution technology, applied in metal material coating process, liquid chemical plating, coating and other directions, can solve the problem of easy rust corrosion, magnetic performance decline or damage, reduce product stability and reliability and other problems, to achieve the effect of good bonding performance, good corrosion resistance, and reducing hydrogen embrittlement.
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Embodiment 1
[0032] Will 2.3 kilograms of high-quality NdFeB permanent magnet materials are first polished in a vibration mill for 2 hours. After degreasing and degreasing with sodium phosphate 20g / liter, sodium carbonate 10g / liter and sodium hydroxide 10g / liter, pickle in 1% nitric acid to remove surface oxides, wash 3 times with water, and then activate copper plating with 5% sulfuric acid . Put the above-mentioned pretreated NdFeB permanent magnet material into the copper plating solution, the composition of the copper plating solution is copper sulfate 0.03 mol / liter, potassium sulfite 0.10 mol / liter, EDTA 0.15 mol / liter, sodium fluoride 0.05 mol / L, pH 6.8. React in a drum for 15 minutes at a temperature of 45°C to form a copper layer on the surface of the NdFeB permanent magnet material. The thickness of the copper layer is 3.5 microns, and the cross file test shows that the copper plating layer does not peel off, does not peel off, and has a good bonding force, see Table 1.
Embodiment 2
[0034] Will 2.5 kilograms of NdFeB permanent magnet materials are polished according to the method in Example 1, degreased and degreased, and activated by pickling. Copper sulfate 0.03 mol / liter, sodium sulfite 0.15 mol / liter, ethylenediamine 0.65 mol / liter, sodium fluoride 0.05 mol / liter, pH 7.5. React in a drum for 25 minutes at a temperature of 45°C to form a copper layer on the surface of the NdFeB permanent magnet material. The thickness of the copper layer is 2.3 microns, and the cross file test shows that the copper plating layer does not peel off, does not peel off, and has a good bonding force, see Table 1.
Embodiment 3
[0036] Will 2.5 kilograms of NdFeB permanent magnet materials are polished according to the method in Example 1, degreased and degreased, and activated by pickling. Copper sulfate 0.03 mol / liter, potassium sulfite 0.10 mol / liter, sodium citrate 0.15 mol / liter, sodium fluoride 0.15 mol / liter, pH 6.9. React at a temperature of 55°C for 15 minutes in a drum to form a copper layer on the surface of the NdFeB permanent magnet material. The thickness of the copper layer is 3.3 microns, and the cross file test shows that the copper plating layer does not peel off, does not peel off, and has a good bonding force, see Table 1.
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