Chinese sapium bark seed extract and preparation method thereof
An extract and seed technology, applied in the field of tallow seed extract and its preparation, can solve the problems of poor tumor effect and the like
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Embodiment 1
[0017] Chinese tallow tree seed powder plus 5 times the amount of 95% ethanol for reflux extraction for 1 hour, the filtered residue plus 4 times the amount of 95% ethanol for reflux extraction for 1 hour, filtered, 4 times the amount and repeated extraction once to combine the filtrate three times, 60 ° C, 700mmHg Recover ethanol, concentrate until there is almost no ethanol smell, add water to 0.8 times the weight of the crude drug, add an equal amount of petroleum ether (60-90°C) for extraction, recover the crude extract after the petroleum ether layer, and the yield is about 40%.
Embodiment 2
[0019] Crude drug powder plus 5 times the amount of 85% ethanol reflux extraction for 1.5 hours, filtered residue plus 4 times the amount of 85% ethanol reflux extraction for 1 hour, filtered, 4 times the amount of repeated extraction once combined filtrate three times, 60C, 700mmHg to recover ethanol , concentrated to almost no ethanol smell, add water to 1.0 times the weight of the crude drug, add an equal amount of petroleum ether (30-60°C) for extraction, recover the crude extract after the petroleum ether layer, and the yield is about 38%.
[0020] Implementation column 3:
[0021] Recipe: Chinese tallow tree seed extract 2.5g
[0022] Lactose 6.0g
[0023] Microcrystalline Cellulose 2.0g
[0024] Magnesium stearate 0.3g
[0025] The above-mentioned ingredients are uniformly mixed to form granules, passed through a 20-80 mesh sieve, dried at 40-80°C, and pressed into tablets.
Embodiment 4
[0027] Recipe: Chinese tallow tree seed extract 2.0g
[0028] Starch 4.0g
[0029] Microcrystalline Cellulose 3.0g
[0031] Mix the above ingredients evenly to make granules, pass through a 20-80 mesh sieve, dry at 40-80°C, and pack into No. 0-3 capsules.
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