Preparation method for cemented carbide mixture
A technology of cemented carbide and mixture, which is applied in the field of preparation of cemented carbide mixture, which can solve the problems of multiple procedures, long process, shortening the preparation process of mixture, etc., and achieve the effect of ensuring uniformity and improving production efficiency
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Embodiment 1
[0015] Example 1: Using medium particle WC powder (FSSS. particle size 4.0 μm, total carbon 6.15%) and cobalt powder (FSSS. particle size 1.5 μm) as the main raw materials, the proportion is 92.0wt% WC+8.0wt% Co, plus 2.0 Wt% Wax, add the alcohol of 250ml / kg mixed material as wet milling medium, add the oleic acid of 0.15wt% in mixed slurry. The above-mentioned substances were ball-milled in a 300L tilting ball mill with a rotation speed of 36 rpm, a filling factor of 0.45, and a ball-to-material ratio of 4:1. After wet milling for 48 hours, the slurry was unloaded and spray-dried and granulated on a BP-300 spray-drying granulator. The test results were:
[0016] The bulk density of the mixture pellets: 3.23g / cm 3 ;
[0017] Hall flow rate: 28.0S / 50g;
[0018] The identification result is:
[0019] Density: 14.71g / cm 3 ; Hardness: HRA89.7;
[0020] Bending strength TRS.: 2860N / mm 2 ; Coercivity Hc: 11.6KA / m;
Embodiment 2
[0022] Example 2: Using fine particle WC powder (FSSS. particle size 1.5 μm, total carbon 6.18%) and cobalt powder (FSSS. particle size 1.5 μm) as the main raw materials, the batching ratio is 94.0wt% WC+6.0wt% Co+0.20wt %TaC, plus 2.2wt% Wax, add 300ml / kg of mixed material alcohol as a wet grinding medium, add 0.15wt% oleic acid and 0.085wt% stearic acid to the mixed slurry. The above-mentioned substances were ball-milled in a 300L tilting ball mill with a rotation speed of 36 rpm, a filling factor of 0.45, and a ball-to-material ratio of 4:1. After 54 hours of wet milling, the slurry was discharged, and spray-dried and granulated on a BP-300 spray-drying granulator. The test results were:
[0023] Bulk density of mixture pellets: 3.70g / cm 3 ;
[0024] Hall flow rate: 20.0S / 50g;
[0025] The identification result is:
[0026] Density: 15.0g / cm 3 ; Hardness: HRA91.8;
[0027] Bending strength TRS.: 2156N / mm 2 ; Coercivity Hc: 18.5KA / m;
[0028] Cobalt Magnetic Com: 5.3...
Embodiment 3
[0029] Example 3: Using fine particle WC powder (FSSS. particle size 16.4 μm, total carbon 6.13%) and cobalt powder (FSSS. particle size 1.5 μm) as the main raw materials, the batching ratio is 84.9wt%WC+15.1wt%Co+0.20wt %TaC, plus 2.0wt% Wax, add 225ml / kg of mixed material alcohol as wet grinding medium, add 0.02wt% oleic acid in the mixed slurry. The above-mentioned substances were ball-milled in a 300L tilting ball mill with a rotation speed of 36 rpm, a filling factor of 0.45, and a ball-to-material ratio of 4:1. After 28 hours of wet milling, the slurry was discharged, and spray-dried and granulated on a BP-300 spray-drying granulator. The test results were:
[0030] The bulk density of the mixture pellets: 3.20g / cm 3 ;
[0031] Hall flow rate: 26.0S / 50g;
[0032] The identification result is:
[0033] Density: 13.83g / cm 3 ; Hardness: HRA84.8;
[0034] Bending strength TRS.: 2120N / mm 2 ; Coercivity Hc: 5.9KA / m;
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Abstract
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