Acidulant for feed and preparation method therefor
A technology of acidifying agent and feed, which is applied in the field of acidifying agent for feed and its preparation, which can solve the problems of large amount of addition, inability to function in the small intestine, and corrosion of machinery, etc., and achieves the effect of low absorption rate and good industrial utilization value
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Embodiment 1
[0021] Mix formic acid and potassium hydroxide in a ratio of 1.55:1.5, slowly add formic acid dropwise to potassium hydroxide, control the reaction temperature at 50-70°C, and continue stirring for 40 minutes after the addition to complete the reaction. Then add the second batch of 1.05 parts of formic acid, control the reaction temperature at 50-80°C, stir for 1 hour, and the reaction product is in a liquid state. Then lower the temperature to 40°C, add citric acid 1 and lactic acid 1 to the reactor according to the recipe, and stir for 20 minutes until the solid citric acid is completely dissolved, so as to avoid the volatilization loss of lactic acid as much as possible, and the obtained liquid mixture is a liquid mixed acidulant.
[0022] Excipient stage: add the liquid mixed acidulant to the excipient silicon dioxide, stir constantly, and the final white powder is the product solid acidulant. The main component of the obtained product is a mixture of lactic acid, citric a...
Embodiment 2
[0025] Mix formic acid and potassium carbonate at a ratio of 1.5:1.45, slowly add formic acid dropwise to potassium carbonate, control the reaction temperature at 50-70°C, and continue stirring for 40 minutes after the addition to complete the reaction. Then add the second batch of 1.0 parts of formic acid, control the reaction temperature at 50-80° C., stir for 1 h, and the reaction product is in a liquid state. Then lower the temperature to 40°C, add citric acid 0.9 and lactic acid 1.1 to the reactor, and stir for 20 minutes until the solid citric acid is completely dissolved, so as to avoid the volatilization loss of lactic acid as much as possible, and the obtained liquid mixture is a liquid mixed acidulant.
[0026] Excipient stage: add the liquid mixed acidulant to the excipient silicon dioxide, stir constantly, and the final white powder is the product solid acidulant. The main component of the obtained product is a mixture of lactic acid, citric acid, formic acid and t...
Embodiment 3
[0029] Mix formic acid and potassium bicarbonate at a ratio of 1.6:1.55, slowly add formic acid dropwise to potassium bicarbonate, control the reaction temperature at 50-70°C, and continue stirring for 40 minutes after the addition to complete the reaction. Then add the second batch of 1.1 parts of formic acid, control the reaction temperature at 50-80°C, stir for 1 hour, and the reaction product is in a liquid state. Then lower the temperature to 40°C, add citric acid 1.1 and lactic acid 0.9 to the reactor, and stir for 20 minutes until the solid citric acid is completely dissolved, so as to avoid the volatilization loss of lactic acid as much as possible, and the obtained liquid mixture is a liquid mixed acidulant.
[0030] Excipient stage: add the liquid mixed acidulant to the excipient silicon dioxide, stir constantly, and the final white powder is the product solid acidulant. The main component of the obtained product is a mixture of lactic acid, citric acid, formic acid ...
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