Ultraviolet curing urethane acrylate adhesive and preparation method thereof

A technology of hydroxypropyl acrylate and isobornyl acrylate, applied in the direction of polyurea/polyurethane adhesives, adhesives, adhesive types, etc., to achieve the effect of short reaction time and low reaction temperature

Inactive Publication Date: 2010-02-17
成都航天明江科技实业有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to overcome the defects of the existing light-curing polyurethane acrylate adhesives, and provide a green, high-performance and non-toxic UV-curable polyurethane acrylate adhesive used in the fields of PDP and the like.

Method used

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Examples

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Effect test

Embodiment Construction

[0018] Below in conjunction with embodiment the present invention will be further described, take the production of 100 kilograms of this product as example.

[0019] 1. Raw materials and their dosage

[0020] Polyether (PPG-2000) 40kg

[0021] Dibutyltin dilaurate 0.1kg

[0022] Toluene diisocyanate (TDI) 7kg

[0023] Isobornyl Acrylate (IBOA) 10kg

[0024] Hydroquinone 0.1kg

[0025] 1,4-butanediol 0.3kg

[0026] Hydroxyethyl Acrylate (HEA) 15kg

[0027] Hydroxypropyl Acrylate (HPA) 21.5kg

[0028] Ethoxylated trimethylolpropane triacrylate (EO-TMPTA) 1kg

[0029] Benzophenone (BP) 2kg

[0030] 1-Hydroxycyclohexylbenzophenone (184) 3kg

[0031] 2. Production process

[0032] 1. Add 40kg of polyether into the reaction kettle, start stirring and heat up to 60°C, then add 0.1kg of dibutyltin dilaurate, and then start to drop 7kg of toluene diisocyanate;

[0033] 2. After adding toluene diisocyanate dropwise, add 10kg of isobornyl acrylate and 0.1kg of hydroquinone, a...

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Abstract

The invention relates to an ultraviolet curing urethane acrylate adhesive and a preparation method thereof, disclosing an approach for obtaining an environment-friendly adhesive. The adhesive is mainly used as a bonding agent for electric products and can be applied to the bonding of PDP displays, LED displays, OLED displays and FPD displays. The adhesive is prepared by using isobornyl acrylate which is an active diluent as a solvent for replacing methylbenzene and benzene, adding toluene diisocynate into polyether, using a chain extender in the reaction, and finishing the reaction within three hours. The adhesive cannot generate poisonous and harmful substances in the processes of production or use and has no pollution to the environment. Meanwhile, the invention has short reaction time and low reaction temperature and can achieve the purpose of energy saving.

Description

Technical field [0001] The invention belongs to the technical field of chemical industry, and is an environment-friendly, low-viscosity, high-efficiency and energy-saving UV curing adhesive. It can be used as an adhesive for electronic appliances, such as the bonding of PDP, LED, OLED, and FPD displays; it can also be used to manufacture optical film materials, such as PET anti-scratch film, anti-reflection film, anti-glare film and isolation film etc. Background technique [0002] At present, the existing photocurable polyurethane acrylate adhesives are mainly used in the manufacture of wood coatings and inks, etc., but its bonding strength, elongation, shrinkage, moisture resistance and electrical properties are not as good as those in the electronics industry. the standard used. With the rapid development of the electronics industry, the demand for high-performance UV-curable adhesives is increasing. However, toxic solvents such as toluene and benzene are often used in...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J175/14C09J175/08
Inventor 陈格德钟安永
Owner 成都航天明江科技实业有限公司
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