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Terpene essence for cigarettes, preparation method and use thereof

A technology for terpenes and cigarettes, used in the preparation of tobacco, essential oils/spice, tobacco, etc., can solve the problems of high reaction temperature, long reaction time, low production efficiency and the like

Active Publication Date: 2010-03-17
HUABAO FLAVOURS & FRAGRANCES CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The production of flavoring essence for tobacco by this method usually has the following defects: 1. Long reaction time, high energy consumption, and low production efficiency; 2. Low product yield and high cost; 3. High reaction temperature and large volatilization loss of aroma components
[0004] At present, how to change the thermal cracking method of terpenoids to produce tobacco flavor technology at home and abroad, to invent a short reaction time, high production efficiency, less energy consumption, low cracking temperature, less volatilization loss of aroma components, high effective content of the product, and low dosage The new method of terpenoid tobacco flavor with few and low cost has not been reported yet; in domestic and foreign patent documents, no literature on producing terpenoid tobacco flavor without thermal cracking method has been found.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0076] Embodiment 1: the preparation of tobacco terpene essence

[0077] The preparation steps are as follows:

[0078] A, preparation of surfactant-coated enzyme:

[0079] (1) Add 0.4 gram of lipase sold under the trade name Lipoxygenase-I by BIOCATALYSTS Company to 250 ml of phosphate buffer (pH7.0), and use an ultrasonic instrument sold under the trade name CQX25-12 by Shanghai Branson Ultrasound Company Sonicate until completely dissolved;

[0080] (2) Add 0.4 g of nonionic surfactant sold by Shanghai Yingzheng Technology Co., Ltd. under the trade name Tween (food grade) to 200 ml of water, and use the same ultrasonic instrument as above to perform ultrasonic treatment until completely dissolved;

[0081] (3) The solution obtained in step (1) and the solution obtained in step (2) were ultrasonically treated and mixed for 25 minutes using the same ultrasonic instrument as above, and then placed in a refrigerator at a temperature of 4 ° C for 24 hours before use;

[0082]...

Embodiment 2

[0087] Embodiment 2: the preparation of tobacco terpene essence

[0088] The preparation steps are as follows:

[0089] The implementation of this example is the same as Example 1, except that 2.50 grams of tobacco terpene complex agent prepared in Example 1, the surfactant-coated enzyme prepared in 0.12 gram of Example 1 are used, at a stirring speed of 200 rpm, the enzyme The solution temperature is 38°C, the pH of the reaction solution is 5.6, and the reaction time is 7h. After the reaction, the reactant is cooled to room temperature to obtain the terpenoid flavor for tobacco.

[0090] According to the ratio of 3 / 10,000 of the total weight of tobacco, the prepared tobacco terpene flavor was added to the 2006 Yunnan B 3 Smoking in shredded tobacco, the results show that the product can effectively improve the aftertaste of the smoke and clean the mouth. At the same time, the product can also play a good role in flavoring, and significantly improve the fullness and coordinat...

Embodiment 3

[0091] Embodiment 3: the preparation of tobacco terpene essence

[0092] The preparation steps are as follows:

[0093] The embodiment of this example is the same as Example 1, except that 1.50 grams of tobacco terpene complex agent prepared in Example 1, the surfactant-coated enzyme prepared in 0.09 gram of Example 1 are used, at a stirring speed of 150 rpm, the enzyme The solution temperature is 38°C, the pH of the reaction solution is 6.0, and the reaction time is 8h. After the reaction is completed, the reactant is cooled to room temperature to obtain the terpenoid flavor for tobacco.

[0094] According to the ratio of 3 / 10,000 of the total weight of tobacco, the prepared tobacco terpene essence was added to the 2006 Shandong B 3 Smoking in shredded tobacco, the results show that this product can effectively cover up the woodiness and green miscellaneous gas in tobacco, reduce the strength, significantly improve the miscellaneous gas, endow tobacco products with a good sw...

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Abstract

The invention relates to terpene essence for cigarettes prepared by utilizing terpene compounds, a preparation method and a use thereof. The preparation method of terpene essence for cigarettes comprises a preparation step of surfactant-coated lipase and an enzymolysis step of terpene compounds. Terpene essence for cigarettes can be used for smoking materials and has a good effect of aromatic flavoring and obviously improves plumpness and harmony of smoke. The method provided by the invention can shorten the reaction time of essence from 10-15 hours to 5-6 hours in a preparation of terpene compounds, reduce the reaction temperature from 120-160 DEG C to 25-40 DEG C, therefore volatilization loss of perfume compounds is reduced from 11-18% to 0.5-1.0% through a thermal cracking method, thequality of products is improved, and meanwhile no discharge of industrial wastes is achieved.

Description

【Technical field】 [0001] The invention relates to the technical field of cigarettes. More specifically, the present invention relates to a terpene flavor for tobacco prepared by using terpene compounds, and also relates to a preparation method of the terpene flavor for tobacco and their use. 【Background technique】 [0002] The aroma, aftertaste, miscellaneous smell, irritation and coordination of smoke are important quality characteristics of tobacco products. The current control methods for these quality indicators at home and abroad are mainly controlled by adding some characteristic compounds. The main trace characteristic compounds in tobacco mainly include ionone, oxo-β-damascenone, macrostigmatrienone, oxidized isophorone, dihydroactinolactone, dihydroactinol, solanone, and norsolanone A series of related compounds such as ketone, isosolone, epoxytheaspirane, theaspirane, dihydrogalalin, oxy-α-ionol acetate, etc. These compounds have played an important role in impr...

Claims

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Application Information

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IPC IPC(8): C11B9/00C12P1/00A24B15/30A24B3/12
Inventor 王希春谷向春
Owner HUABAO FLAVOURS & FRAGRANCES CO LTD
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