Coloring combination, color filter and color liquid crystal display element
A coloring composition and coloring agent technology, applied in the direction of instruments, optical filters, optics, etc., can solve the problems of difficulty in achieving high contrast, poor storage stability of coloring compositions, and inability to obtain sufficient contrast ratio, etc., to achieve high preservation The effect of stability
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[0236] [Example]
[0237] Examples are given below to more specifically describe the embodiments of the present invention. However, the present invention is not limited by the following examples.
[0238] Dispersant analysis
[0239] Dispersant B1
[0240] Dispersant B1 is a commercially available product of pigment wetting and dispersing agent. It is a modified acrylic block copolymer of propylene glycol methyl ether acetate / butyl cellosolve = 1 / 1 (mass ratio) solution (solid content concentration 40% by mass) , Acid value = 0). Through thermal decomposition GC-MS, FT-IR measurement, and proton NMR, it was confirmed that the dispersant B 1 contained the methacryloxy ethyl benzyl dimethyl ammonium chloride and dimethyl amino ethyl methacrylate The A block of the repeating unit, and has methacrylic acid from methyl methacrylate, butyl methacrylate, 2-ethylhexyl methacrylate, benzyl methacrylate and triethylene glycol ethyl ether A block copolymer of the B block of the ester repeat...
Example Embodiment
[0253] Preparation Example 1
[0254] (A) 15 parts by mass of CI Pigment Red 254 (manufactured by チバスペシャリティケミカルズ, trade name BK-CF) as the colorant (A), and 3 parts by mass (calculated as solid content) as the specific dispersant of the dispersant (B) That is, dispersant B1, propylene glycol monomethyl ether acetate / propylene glycol monoethyl ether = 90 / 10 (mass ratio) mixed solvent as a solvent, and the mixed solvent is used in an amount such that the solid content concentration is 20% by mass, The mixture was mixed and dispersed in a bead mill for 12 hours to prepare a colorant dispersion liquid (M-1).
Example
[0255] Preparation examples 2-13
[0256] Except that the colorant and the dispersant were changed as shown in Table 1 in Preparation Example 1, colorant dispersion liquids (M-2) to (M-15) were prepared in the same manner as Preparation Example 1.
[0257]
[0258] In Table 1, "R254" refers to CI Pigment Red 254, "R177" refers to CI Pigment Red 177, "Y150" refers to CI Pigment Yellow 150, "Y139" refers to CI Pigment Yellow 139, "G36" "Refers to CI Pigment Green 36, "B15:6" refers to CI Pigment Blue 15:6, and "V23" refers to CI Pigment Violet 23.
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