Preparation method of cationic dyeable halogen-free flame retardant polyester fiber
A flame-retardant polyester and cationic technology, applied in the direction of single-component copolyester artificial filaments, etc., can solve the problems of cationic dyeability decline, cost increase, and more by-products, and achieve significant flame retardancy and cationic dyeability. Dyeing effect, production cost reduction, product performance improvement effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0019] Step 1. Synthesis of cationically dyeable and flame retardant compound
[0020] Sodium isophthalate sulfonate, 2-carboxyethyl hypophosphorous acid (CEPPA) and deionized water in a molar ratio of 1:1.5:10 were added to a glass reaction vessel, heated to 50°C in a water bath, reacted for 1 hour, and waited for After the reaction is completed, the reaction product is filtered out, and dried at a temperature of 110-150° C. to obtain a cationically dyeable flame-retardant compound.
[0021] Step 2. Synthesis of cationically dyeable halogen-free flame retardant polyester chips
[0022] Terephthalic acid (PTA), step 1 product and ethylene glycol (EG) are in a molar ratio of 1: 0.02: 1.15, are added to the esterification kettle, and the esterification kettle is stirred and heated to 230 ° C, and the interior of the esterification kettle is controlled The pressure reaches 200kPa, react for 1 hour, make the esterification rate reach more than 90%, end the esterification, release...
Embodiment 2
[0026] Step 1. Synthesis of cationically dyeable and flame retardant compound
[0027] Sodium isophthalate sulfonate, 2-carboxyethyl hypophosphorous acid (CEPPA) and deionized water in a molar ratio of 1:2:20 were added to a glass reaction vessel, heated to 60°C in a water bath, reacted for 3 hours, and waited for After the reaction, the reaction product was filtered out, and dried at 130° C. to obtain a cationically dyeable flame retardant compound.
[0028] Step 2. Synthesis of cationically dyeable halogen-free flame retardant polyester chips
[0029] Terephthalic acid (PTA), step 1 product and ethylene glycol (EG) are in a molar ratio of 1: 0.04: 1.2, are added to the esterification kettle, and the esterification kettle is stirred and heated to 240 ° C, and the interior of the esterification kettle is controlled The pressure reaches 300kPa, the reaction is performed for 1.5 hours, the esterification rate reaches more than 95%, the esterification is completed, the pressure ...
Embodiment 3
[0033] Step 1. Synthesis of cationically dyeable and flame retardant compound
[0034] Sodium isophthalate sulfonate, 2-carboxyethyl hypophosphorous acid (CEPPA) and deionized water in a molar ratio of 1:2.5:30 were added to a glass reaction vessel, heated to 80°C in a water bath, reacted for 5 hours, and waited for After the reaction was completed, the reaction product was filtered out and dried at 150° C. to obtain a cationically dyeable flame retardant compound.
[0035] Step 2. Synthesis of cationically dyeable halogen-free flame retardant polyester chips
[0036]Terephthalic acid (PTA), step 1 product and ethylene glycol (EG) are in a molar ratio of 1: 0.08: 1.25, are added to the esterification kettle, and the esterification kettle is stirred and heated to 250 ° C, and the interior of the esterification kettle is controlled The pressure reaches 400kPa, and the reaction is carried out for 2 hours to make the esterification rate reach more than 99% to complete the esterif...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com