Vitamin E and organic germanium composite core-containing microcapsule finishing agent and preparation and application thereof

A technology of microcapsule finishing and organic germanium, which is applied in the direction of microcapsule preparation, microsphere preparation, fiber treatment, etc., can solve the problems of dry skin, rough skin, excessive aging, etc., and achieve anti-aging, high added value, and high-efficiency anti-oxidation Effect

Inactive Publication Date: 2011-04-06
DONGHUA UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Lack of it will have adverse consequences suc

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] The salad oil, vitamin E and organic germanium were weighed respectively and stirred evenly under a magnetic stirrer to obtain a compound oil; the organic germanium content in the compound oil was 0.01%, and the vitamin content was E5%.

[0030] Weigh 10 grams of compound oil and add it into a three-necked bottle, add 2.1% of the weight of the compound oil Span 60 and 2.9% of Tween 60, heat up to 30-50 degrees under stirring conditions, and add 0-3% anion high 85 grams of aqueous solution of molecular emulsion stabilizer CMC is added dropwise to the oil phase at a certain speed, and the compound oil is emulsified in water under magnetic stirring, and the mechanical emulsification time is 2-4 hours.

[0031] Weigh 37 grams of melamine-formaldehyde prepolymer (80% solid content) and add it to the above emulsion, add 5% citric acid dropwise at a rate of 0.5mL / min to adjust the pH to 3.5-4, heat to 60°C, and keep warm for 1h. Then the temperature was raised to 90°C, and the...

Embodiment 2

[0033] The olive oil, vitamin E and organic germanium were weighed and stirred evenly under a magnetic stirrer to obtain a compound oil; the content of organic germanium in the compound oil was 0.8%, and the content of vitamin E was 10%.

[0034] Weigh 10 grams of compound oil and add it into a three-necked bottle, add 2.1% of the weight of the compound oil Span 60 and 2.9% of Tween 60, heat up to 30-50 degrees under stirring conditions, and add 0-3% anion high 85 grams of aqueous solution of molecular emulsion stabilizer CMS is added dropwise to the oil phase at a certain speed, and the compound oil is emulsified in water under magnetic stirring, and the mechanical emulsification time is 2-4 hours.

[0035] Weigh 19 grams of melamine-formaldehyde prepolymer (80% solid content) and add it to the above emulsion, add 5% citric acid dropwise at a rate of 0.5mL / min to adjust the pH value to 3.5-4, heat to 60°C, and keep warm for 0.5h , and then the temperature was raised to 90°C, ...

Embodiment 3

[0037] Cotton fabric vitamin E / organic germanium composite microcapsule finishing process:

[0038] Process prescription: 30g of microcapsule finishing in Example 1

[0039] Low temperature adhesive (40%) 45g

[0040] water x

[0041] Total: 1000g

[0042] Process flow:

[0043] Cotton fabric--padding (rolling liquid rate 130%)--hot air drying--baking at 120 degrees for 3 (min)--finished product.

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Abstract

The invention relates to a vitamin E and organic germanium composite core-containing microcapsule finishing agent and preparation and application thereof. The vitamin E and organic germanium composite core-containing microcapsule finishing agent comprises the following components: more than 0 and less than or equal to 10 percent of vitamin E and more than 0 and less than or equal to 8 percent of organic germanium. The preparation comprises the following steps of: uniformly stirring oil, the vitamin E and the organic germanium to obtain a composite oil core; adding a surfactant into the composite oil core, and heating to the temperature of between 30 and 50 DEG C under stirring; adding aqueous solution comprising 0 to 3 percent of anionic polymer emulsion stabilizer dropwise, and emulsifying composite oil in water under stirring; and adding the prepolymer of melamine formaldehyde into the emulsified system, adjusting the pH value of the solution to be 3.5 to 4, reacting and adjusting the pH value to 9 to obtain the vitamin E and organic germanium composite core-containing microcapsule finishing agent. The microcapsule finishing agent has the effects of effective antioxidation, improvement on skin blood circulation, enhancement of skin cell viability and anti-aging of the vitamin E and also has the function of enhancement of human immunoregulation of the organic germanium.

Description

technical field [0001] The invention belongs to the field of fabric microcapsule finishing agent, preparation and application, in particular to a fabric finishing agent with vitamin E and organic germanium composite core material, preparation and application. Background technique [0002] In the history of human development, textiles firstly take heat preservation as their main function. With the development and progress of society, textiles are combined with lifestyle and quality, and popular colors and styles emerge in endlessly. In this colorful textile In the market, the emergence of health care textiles has attracted more and more attention. [0003] The so-called health-care textiles are to arrange the health-care substances on the clothes, and then release them slowly. Through the direct contact between the clothes and the skin, the health-care substances penetrate into the pores of the skin and are absorbed by the human body, supplementing various substances needed b...

Claims

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Application Information

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IPC IPC(8): D06M23/12D06M13/51D06M13/152B01J13/02
Inventor 闵洁侯世清陈伟严瑞祥刘宝江杨卓
Owner DONGHUA UNIV
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