Manufacturingmethod of active humic acid controlled-release fertilizer

The technology of active humic acid and production method is applied in the production field of active humic acid slow-release fertilizer, which can solve the problems of high cost and large pollution, and achieve the effects of low production cost, good effect and large space for total nutrient change.

Active Publication Date: 2011-05-25
SHANDONG AGRI UNIV FERTILIZER TECH CO LTD
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AI Technical Summary

Problems solved by technology

[0005] In order to solve the problem of large pollution and high cost of conventional humic acid activation technology, the present invention provides a production method of active humic acid slow-release fertilizer, and invents the activation of humic acid and organic combination with the production of compound fertilizer, the activation rate of humic acid is high, Low production cost, simple operation process, suitable for existing compound fertilizer enterprises to use existing equipment for large-scale production, and solve the disadvantages of large pollution, high cost and low content of active humic acid in conventional production

Method used

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  • Manufacturingmethod of active humic acid controlled-release fertilizer
  • Manufacturingmethod of active humic acid controlled-release fertilizer
  • Manufacturingmethod of active humic acid controlled-release fertilizer

Examples

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specific Embodiment approach 1

[0027] A preparation method of active humic acid slow-release fertilizer (26-6-6), comprising the following steps:

[0028] a, pulverization of weathered coal raw materials: input weathered coal raw materials (total humic acid content 50%) into the ball mill, and pulverize the raw materials to a particle size of 80 mesh;

[0029] b, urea melting: powdery or small granular urea is input into the urea-based melting tank, as shown in Table 2: 100 parts by mass of urea is added to 15 parts by mass of water, and 20 parts by mass of powdered potassium chloride is added, and the steam pan is used to Heat the tube to 110°C and stir to make urea-potassium chloride eutectic to form urea liquid;

[0030] c. Humic acid activation: Add the weathered coal raw material prepared in a into another reaction tank, and add a certain amount of sodium hydroxide according to the total humic acid content in the weathered coal, the mass parts of humic acid and sodium hydroxide The ratio is 100:17, th...

specific Embodiment approach 2

[0038] A preparation method of active humic acid slow-release fertilizer (15-17-13), comprising the following steps:

[0039] a, pulverization of lignite raw material: input lignite raw material (total humic acid content 55%) in ball mill, raw material is pulverized to particle size 100 orders;

[0040] b, urea melting: powdery or small granular urea is input into the urea-based melting tank, as shown in Table 2: 100 parts by mass of urea is added to 5 parts by mass of water, and 15 parts by mass of powdered potassium chloride is added, and the steam pan is used to Heat the tube to 130°C and stir to make urea-potassium chloride eutectic to form urea liquid;

[0041] C, humic acid activation: the lignite raw material prepared in a is added in another reaction tank, and a certain amount of sodium hydroxide is added according to its total humic acid content in the lignite, and the mass and number ratio of humic acid and sodium hydroxide is 100:17, detect the urea content in the ...

specific Embodiment approach 3

[0048] A preparation method of active humic acid slow-release fertilizer (14-0-18), comprising the following steps:

[0049] a, pulverization of the mixed coal raw material of weathered coal and lignite: input the mixed raw material of weathered coal and lignite (60% of total humic acid content) into the ball mill, and pulverize the raw material to a particle size of 150 mesh;

[0050] b, urea melting: powdery or small granular urea is input into the urea-based melting tank, as shown in Table 2: 100 parts by mass of urea is added to 10 parts by mass of water, and 18 parts by mass of powdered potassium chloride is added, and the Heat the tube to 120°C and stir to make urea-potassium chloride eutectic to form urea liquid;

[0051]c, humic acid activation: put the coal raw material prepared in a into another reaction tank, and add a certain amount of sodium hydroxide according to its total humic acid content in the coal, and the mass-number ratio of humic acid and sodium hydroxid...

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Abstract

The invention discloses a manufacturing method of active humic acid controlled-release fertilizer, comprising the following steps: taking weathered coal or lignite as raw materials; adopting the production equipment of compound fertilizer; taking sodium hydroxide and urea as an activator; in an activating reaction jar, activating and converting humic acid in the weathered coal or lignite by fusedurea liquid and sodium hydroxide to form the urea liquid containing the active humic acid; producing by combing with the compound fertilizer; injecting the urea liquid containing the active humic acid onto the compound fertilizer material in a granulation barrel to round and granulate; and drying, and screening to obtain the black, light and round humic acid controlled-release fertilizer product of different content proportions. In the manufacture scheme, the humic acid urea activating liquid has the following raw materials at the ratio of urea to humic acid to potassium chloride to water tosodium hydroxide of 100:100:(15-200):(5-15):(7-12), and other solid granulation raw materials (comprising urea, monoammonium phosphate, potassium chloride, ammonium sulphate, bentonite and the like) are designed according to nutrient content proportions of different fertilizers. In the manufacture method, humic acid activation and compound fertilizer production are organically combined and are carried out simultaneously, and thus the manufacture method has the characteristics of simple operation process, low cost, large production capability, black, light and round product particle, efficient controlled release of the nutrient, high utilization ratio, wide market prospect and the like, can greatly improve the yield and the quality of crop and improves fertilization soil.

Description

1: Technical field [0001] The invention relates to a method for preparing a humic acid slow-release fertilizer, in particular to a method for making an active humic acid slow-release fertilizer with weathered coal or lignite as raw materials and different active humic acid contents and nutrient contents. Two: background technology [0002] Humic acid has a wide range of uses and has been used in various aspects such as industry, agriculture, medicine, and environmental protection. In terms of fertilizer utilization, as early as the late 1950s, there were reports in foreign countries that combined humic acid and urea to produce fertilizers. In particular, Japan began to nitrate humic acid and urea to produce nitrohumic acid urea in the 1960s. In addition, the former Soviet Union, India, etc. also have similar research. However, industrial production has not been carried out. [0003] my country's humic acid resources are very rich. Since the 1970s, the development of humic a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C05G3/00
Inventor 丁方军吴钦泉孟庆羽陈士更马玉增谷端银
Owner SHANDONG AGRI UNIV FERTILIZER TECH CO LTD
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