Visual gas hydrate experimental device

A gas hydrate and experimental device technology, applied in measurement devices, chemical method analysis, instruments, etc., can solve problems such as small visual range and small reaction volume, and achieve the goal of overcoming short bubble travel, increasing gas-liquid contact area, and increasing The effect of gas solubility

Active Publication Date: 2011-08-03
GUANGZHOU INST OF ENERGY CONVERSION - CHINESE ACAD OF SCI
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  • Abstract
  • Description
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AI Technical Summary

Problems solved by technology

[0005] The problem to be solved by the present invention is to provide a visual gas hydrate experimental device that overcomes the above-mentioned shortcomings of the existing hydrate formation experimental devices such as small reaction volume and small visual range.

Method used

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Embodiment Construction

[0024] The preferred embodiments of the present invention will be described in further detail below in conjunction with the accompanying drawings.

[0025] attached figure 1 The marks in each are: 1. Gas cylinder, 2. Liquid tank, 3. Mass flow controller and integrator, 4. Metering pump, 5. Refrigeration system, 6. Heat exchanger, 7. Constant temperature water tank, 8. Static mixing Device, 9, water jacket, 10, distributor, 11, reactor, 12, pressurized water pump, 13, safety valve, 14, vacuum pump, 15, PID pressure regulating valve, 16, gas-liquid separator, 17, gas phase Chromatograph, 18, automatic gas sampler, 19, gas cylinder, 20, computer, 21, data acquisition card, 22, pressure reducing valve, 23, window. V1~V29 are all valves, except check valve V24 and check valve V25, the rest are stop valves.

[0026] Such as figure 1 As shown, the visualized gas hydrate experimental device of the present invention includes a visualized hydrate reactor, a steady flow gas supply, a ...

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Abstract

The invention discloses a visual gas hydrate experimental device. The visual gas hydrate experimental device comprises a reactor, a constant-current gas supply system, a constant-current liquid supply system, a temperature control system, a constant-pressure gas exhaust system, a sampling analysis system and a data acquisition and processing system, wherein the reactor is divided into a plurality of sections; each section is provided with a window; a water jacket is arranged on an external wall without the window; a feeding hole is formed at the bottom; the constant-current gas supply system and the constant-current liquid supply system supply gas and a solution to the reactor respectively at a constant speed; the temperature control system controls the gas and the solution which are to be supplied to the reactor and controls a temperature of each water jacket; the constant-pressure gas exhaust system is used for exhausting the gas from the reactor and controlling a pressure in the reactor to be constant; the sampling analysis system takes samples from the interior of the reactor and carries out component analysis; and the data acquisition and processing system acquires the data of the constant-current gas supply system, the constant-current liquid supply system, the reactor and the temperature control system and carries out analysis. By adoption of the scheme, fast and efficient generation of a gas hydrate can be realized, on-line real-time observation of the crystal structure and the appearance of the hydrate in the process of hydrate composition / decomposition can be also realized, and the crystal structure and the appearance of the hydrate are analyzed by image processing software.

Description

technical field [0001] The invention relates to a gas hydrate experimental device, in particular to an experimental device which can be used for multi-component mixed gas hydrate formation / decomposition kinetics, hydrate crystal structure and morphology determination. Background technique [0002] Gas hydrate (hereinafter referred to as hydrate) is composed of water and CH 4 、C 2 h 6 , CO 2 or H 2 The non-stoichiometric clathrate crystalline substance formed by small molecule gases such as S under high pressure and low temperature environment is also called clathrate hydrate. The host water molecules are connected by hydrogen bonds to form some polyhedral cages, and guest molecules of appropriate size can be filled in these cages to make them thermodynamically stable. Gas hydrate has a strong gas storage capacity, and can store 160-180m3 per cubic meter 3 Gas, and solid, easy to transport. Gas hydrate technology has broad application prospects. In addition to natural ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N31/00
Inventor 李小森吕秋楠陈朝阳李刚曾志勇张郁颜克凤
Owner GUANGZHOU INST OF ENERGY CONVERSION - CHINESE ACAD OF SCI
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