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Method for preparing nitrogen-doped graphene material with hydrothermal process

A technology of nitrogen-doped graphene and hydrothermal method, which is applied in the field of preparation of nitrogen-doped graphene materials, can solve the problems of complex equipment required for the reaction, difficult control of nitrogen content, and difficulty in industrial production, and achieve easy industrial production, The effect of low production cost and simple equipment

Inactive Publication Date: 2013-02-06
HEILONGJIANG UNIV
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  • Application Information

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Problems solved by technology

[0004] The present invention aims to solve technical problems such as low nitrogen content, difficult control of nitrogen content, high production cost, complex equipment required for reaction, harsh reaction conditions, low output and difficulty in industrialized production existing in the existing preparation method of nitrogen-doped graphene material; Thereby providing a method for preparing nitrogen-doped graphene materials by hydrothermal method

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  • Method for preparing nitrogen-doped graphene material with hydrothermal process
  • Method for preparing nitrogen-doped graphene material with hydrothermal process

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specific Embodiment approach 1

[0012] Specific embodiment one: the method for preparing nitrogen-doped graphene material by hydrothermal method in this embodiment is completed by the following steps: one, add graphite oxide in the solvent, then add surfactant, then use ultrasonic method or heating Mix uniformly by stirring to obtain mixture A, wherein the solvent is one or a mixture of several of water, methanol, ethanol, ethylene glycol, N,N-dimethylformamide, and the graphite oxide The mass ratio with solvent is 1:100~2000, and the mass ratio of described surfactant and graphite oxide is 0.01~50:1; Two, then add nitrogen-containing compound in mixture A, wherein nitrogen-containing compound and graphite oxide The mass ratio is 10 to 500:1, and then the mixture is uniformly mixed by ultrasonic method or heating and stirring method to obtain the mixture B; 3. The mixture B is subjected to hydrothermal reaction, the hydrothermal reaction temperature is 100~190°C, and the hydrothermal reaction time is 4-48 ho...

specific Embodiment approach 2

[0015] Specific embodiment two: the difference between this embodiment and specific embodiment one is: the surfactant described in step one is cationic surfactant, anionic surfactant, nonionic surfactant and amphoteric surfactant A sort of. Other steps and parameters are the same as in the first embodiment.

specific Embodiment approach 3

[0016] Specific embodiment three: this embodiment is different from specific embodiment two in that: the cationic surfactant is cetyl trimethyl ammonium bromide, cetyl dimethyl benzyl ammonium bromide, Cetyl alcohol polyoxyethylene ether group dimethyl octyl ammonium chloride, lauryl alcohol polyoxyethylene ether group dimethyl methyl ammonium chloride, octylphenol polyoxyethylene ether group dimethyl decyl bromide ammonium chloride, octylphenol polyoxyethylene ether dimethyl decyl ammonium chloride or cetyl alcohol polyoxyethylene ether dimethyl octyl ammonium chloride. Other steps and parameters are the same as in the second embodiment.

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Abstract

The invention discloses a method for preparing a nitrogen-doped graphene material with a hydrothermal process, relating to a method for preparing the nitrogen-doped graphene material. The technical problems of lower nitrogen content, difficulty in control of nitrogen content, high production cost, complex structure of equipment required by reaction, rigorous reaction conditions, low yield, difficulty in industrialized production and the like in the traditional method for preparing the nitrogen-doped graphene material are solved in the invention. The method comprises the steps of: 1, dissolving graphite oxide in a solvent, adding a surfactant and uniformly mixing; 2, adding a nitrogen-containing compound, and uniformly mixing; and 3, after a hydro-thermal reaction, washing and drying to obtain the nitrogen-doped graphene material. The nitrogen-doped graphene material prepared in the invention has the advantages of higher nitrogen content, controllable nitrogen content, low production cost, simple structure of required equipment, high yield and easiness in realizing industrialized production.

Description

technical field [0001] The invention relates to a preparation method of a nitrogen-doped graphene material. Background technique [0002] Graphene with a two-dimensional structure has excellent physical and chemical properties, and has important application value in fields such as field emission transistors, supercapacitors, and lithium-ion batteries. However, nitrogen doping is very important for tuning the electronic structure of graphene. Nitrogen-doped graphene has important applications in supercapacitors, fuel cells and other fields. Therefore, in order to meet the needs of different fields, the design and synthesis of nitrogen-doped two-dimensional materials is very necessary. The traditional method for preparing nitrogen-doped graphene mainly contains: (1) in the process of preparing graphene by chemical vapor deposition (CVD), feed ammonia gas simultaneously and carry out nitrogen doping, and the highest nitrogen content is 5%; ( 2) In the process of preparing gr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B31/04
Inventor 付宏刚孙立王蕾田春贵穆光田国辉
Owner HEILONGJIANG UNIV
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