Energy-saving process for producing melamine

A technology for melamine and production process, which is applied in the field of energy-saving melamine production process, can solve the problems affecting the operation period of the device, the temperature difference between liquid and urine is large, easy to block or form walls, etc. small effect

Inactive Publication Date: 2012-05-16
郗运柱
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage of this process is that the air-conditioning fan pressurizes the high-temperature gas, which requires a large fan power and high energy consumption; the temperature difference between the liquid and urine in the liquid and urine washing tower changes greatly, and it is easy to block or form walls, block the liquid and urine nozzle, and affect the device. run cycle

Method used

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  • Energy-saving process for producing melamine
  • Energy-saving process for producing melamine

Examples

Experimental program
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Effect test

Embodiment 1

[0010] Example 1: Using urea as a raw material, in a reactor, through the catalytic action of a catalyst, melamine, ammonia and carbon dioxide are reacted at 350°C and a pressure of 0.8MPa, and the material gas coming out of the reactor enters a hot gas cooler, and the cooled The hot process gas enters the filter for filtration, the filtered process gas containing melamine enters the crystallizer, the crystallized melamine enters the cyclone separator, and the separated solid melamine is sent to the bin for packaging, and the gas from the cyclone separator enters the heat exchange The device uses water to cool the gas containing ammonia and carbon dioxide at 200°C to 135°C, then enters the liquid urine scrubber to purify the process gas, and the purified and absorbed gas passes through the separator to separate the liquid urine droplets entrained in the gas. The separated gas is divided into three paths: one path is compressed by a compressor and enters the reactor, one path is...

Embodiment 2

[0011] Example 2: Using urea as a raw material, in the reactor through the catalysis of the catalyst, melamine, ammonia and carbon dioxide are reacted at 380°C and 1MPa pressure, and the material gas coming out of the reactor enters the hot gas cooler, and the cooled heat The process gas enters the filter for filtration, the filtered process gas containing melamine enters the crystallizer, the crystallized melamine enters the cyclone separator, the separated solid melamine is sent to the bin for packaging, and the gas from the cyclone separator enters the heat exchanger , the gas containing ammonia and carbon dioxide at 210°C is cooled to 140°C by water, and then enters the liquid urine washing tower to purify the process gas, and the purified and absorbed gas passes through the separator to separate the liquid urine droplets entrained in the gas, and separates The final gas is divided into three routes: one is compressed by a compressor and enters the reactor, the other is boo...

Embodiment 3

[0012] Example 3: Using urea as a raw material, in the reactor through the catalysis of the catalyst, melamine, ammonia and carbon dioxide are reacted at 400 ° C and 1.2 MPa pressure, and the material gas coming out of the reactor enters the hot gas cooler, and the cooled The hot process gas enters the filter for filtration, the filtered process gas containing melamine enters the crystallizer, the crystallized melamine enters the cyclone separator, and the separated solid melamine is sent to the bin for packaging, and the gas from the cyclone separator enters the heat exchange The gas containing ammonia and carbon dioxide at 210°C is cooled down to 140°C by water, and then enters the liquid urine washing tower to purify the process gas, and the purified and absorbed gas passes through the separator to separate the liquid urine droplets entrained in the gas. The separated gas is divided into three paths: one path is compressed by a compressor and enters the reactor, one path is ...

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PUM

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Abstract

The invention relates to an energy-saving process for producing melamine, comprising the following steps: using urea as the raw material, and producing melamine, ammonia and carbon dioxide in a reactor under the catalytic function of a catalyst at 350-420 degrees centigrade and a pressure of 0-1.5 MPa through reaction, wherein material gas from the reactor enters a hot-gas cooler, and the cooled hot technological gas enters a filter to be filtered, and the filtered technological gas containing melamine enters a crystallizer, and the melamine after crystallization enters a cyclone separator, and the separated solid triamine is sent to a storage bin to be packaged, and the gas coming out from the cyclone separator enters a heat exchanger; cooling the gas containing ammonia and carbon dioxide at about 200-220 degrees centigrade by water to about 30-145 degrees centigrade, and purifying the technological gas in an urine liquid washing tower; separating urine liquid fog drops carried in the purified gas by a separator, wherein the gas after separation is divided into three ways: one way gas is compressed into the reactor by the compressing machine, and one way gas enters the crystallizer by a cool air fan through pressure boosting to be used as cool air, and one way is a tail gas exhaust system for other purposes. The process disclosed by the invention has characteristics of compact equipment, simple technology, less energy consumption, cost saving and so on.

Description

technical field [0001] The invention relates to an energy-saving melamine production process. Background technique [0002] The current production process of melamine uses liquid urea as the raw material. In the fluidized bed reactor, it reacts at 350-420°C and 0-1.5MPa pressure to form melamine, ammonia and carbon dioxide. The material gas from the reactor enters the hot gas. Cooler, gasification and cooling, so that the high boiling point by-products are crystallized as solids, the cooled process material gas enters the hot gas filter to filter the solid impurities in the gas, and the filtered gas enters the crystallizer and comes from the liquid urine washing system The process cold air is reverse contact heat exchange, melamine is precipitated from the process material gas in the form of solid, and then the gas containing melamine solid is separated by the cyclone separator and sent to the packaging system. The gas from the cyclone separator is pressurized by the fan an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D251/60
CPCY02P20/10
Inventor 郗运柱
Owner 郗运柱
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