Method for obtaining high-purity zinc by electrolyzing zinc chloride
A zinc chloride, high-purity technology, applied in the direction of photography technology, equipment, photography auxiliary technology, etc., to achieve the effect of solving post-processing problems
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Embodiment 1
[0031] 1. Put 80g of ammonium chloride and 100g of sodium chloride into a beaker respectively, stir and dissolve with deionized water.
[0032] 2. Dissolve 160 grams of zinc chloride in the above conductive saline solution.
[0033] 3. Use such as figure 1 In the shown electrolysis system device, the solution in the beaker is transferred to a large volume cylinder of 1L and then poured into a 1L plexiglass buffer tank 14 .
[0034]4. Use a zinc sheet with a Zn99.99% content as an anode of 30×40mm, and a 30×40mm polished pure aluminum sheet as a cathode, and turn on a 0.02A direct current to electrolyze the above electrolyte for 1 hour.
[0035] 5. Use a peristaltic pump to inject the electrolyte after electrolytic treatment with a small current into a 300mL glass electrolytic cell 1, use a RuTi-coated DSA anode of 40×60mm, a polished aluminum cathode of 40×60mm, and control the electrode distance to 4cm, and pass 2A DC current for electrolysis .
[0036] 6. After 1 hour of ...
Embodiment 2
[0054] 1. Put 80g of ammonium chloride and 100g of sodium chloride into a beaker respectively, stir and dissolve with deionized water.
[0055] 2. Dissolve 160 grams of zinc chloride in the above conductive saline solution.
[0056] 3. Use such as figure 1 In the shown electrolysis system device, the solution in the beaker is transferred to a large volume cylinder of 1L and then poured into a 1L plexiglass buffer tank 14 .
[0057] 4. Use a zinc sheet with a Zn99.99% content as an anode of 30×40mm, and a 30×40mm polished pure aluminum sheet as a cathode, and turn on a 0.02A direct current to electrolyze the above electrolyte for 1 hour.
[0058] 5. Use a peristaltic pump to inject the electrolytic solution after low-current electrolysis treatment into the 300mL glass electrolytic cell 1, use RuTi-coated DSA anode 40×60mm, use Zn99.99% zinc sheet cathode 40×60mm, and control the electrode distance to 4cm , Through 2A DC current electrolysis.
[0059] 6. After 1 hour of elect...
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