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Method for preparing high-purity dipping asphalt

A bitumen, high-purity technology, applied in the processing of tar pitch/petroleum pitch/natural pitch by distillation, and the processing of tar pitch/petroleum pitch/natural pitch by selective extraction, which can solve the problem of high energy consumption, low output and high manufacturing cost problem, to achieve the effect of simple process steps, high purity and low manufacturing cost

Inactive Publication Date: 2012-06-13
韩国清
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the high manufacturing cost and low output of high-purity impregnated asphalt products, most industries use ordinary medium-temperature coal tar pitch instead, resulting in low product quality, high energy consumption, and poor quality. It is difficult to meet high use requirements and hinder the metallurgical industry. , electronics industry, new energy and other industries product upgrades

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0010] The embodiment that the inventive method prepares high-purity impregnated bitumen is as follows:

[0011] Use an asphalt pump to pump liquid medium-temperature asphalt from the raw material tank to 13m 3 The mixing tank with temperature control and stirring is up to 5T, and then the gear pump is used to pump the pre-prepared quenching agent (60% washing oil: diesel oil 40%) 5T from the quenching agent storage tank into the mixing tank. Under certain conditions, turn on the mixer and stir for 1.5 hours to achieve a fully mixed reaction, fully quench, and then use a pump to pump the mixed solution into a volume of 30m 3 After standing still at 140°C to 150°C for 24 hours, take the middle and upper layer liquid for analysis. After the content of quinoline insolubles reaches the standard, open the liquid level control valve of the corresponding liquid level and pump in a volume of 13m 3 The automatic temperature-controlled stirring still kettle, the temperature is raised t...

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PUM

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Abstract

The invention, relating to the preparation technique of asphalt materials, particularly discloses a method for preparing high-purity dipping asphalt. The method comprises the following steps: step 1, preparing an extracting agent by mixing 57-63 wt% of washing oil and 37-43 wt% of diesel oil; step 2, putting middle-temperature liquid asphalt and the extracting agent in a mixing kettle according to the weight ratio of 1:1, stirring for 1.5-2 h at a kettle temperature of 148-152 DEG C, then pumping into a standing settler, standing for more than 24 h at a temperature of 140-150 DEG C, and pumping into the asphalt liquid having a required purity in a distilling still; step 3, steaming out distillates of the extracting agent by using an underpressure distillation method, and finally carrying out cooling forming by a forming machine. A product obtained by the invention has high purity, wherein the content of quinoline insolubles is generally less than 0.5 %, and the minimum content can be less than 0.1 %, and the product can satisfy the high request for utilization, and the steps are simple, and the preparation cost is low.

Description

technical field [0001] The invention relates to the manufacturing technology of asphalt materials, in particular to a preparation method of high-purity impregnated asphalt. Background technique [0002] At present, in graphite products, electric carbon products, electronics industry, new energy and other industries, there is an urgent need for high-quality impregnated pitch. [0003] High-purity impregnated asphalt is a high-purity asphalt obtained by separating out quinoline insoluble matter under a certain working temperature process condition with medium-temperature asphalt as raw material. It has a wide range of uses and is important. Densifying and reinforcing agent for plain products is an important basic material, widely used in metallurgy, electronics, machinery, aerospace, new energy development, nuclear industry, medicine, military industry and other fields, for example: 1. It is indispensable for power lithium batteries The missing raw material; 2. It is a densif...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10C3/08C10C3/06
Inventor 韩国清
Owner 韩国清
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