Normal temperature solidified thermosetting epoxy bitumen material and preparation method thereof
An epoxy asphalt material, curing technology at room temperature, applied in building insulation materials, building components, buildings, etc., can solve the problems of operating workers' health and atmospheric environment hazards, long curing time, high curing temperature, etc., to reduce energy consumption and high temperature Hazard, reduce the risk of volatilization, the effect of mild preparation conditions
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Embodiment 1
[0026] formula:
[0027] Part A: Bisphenol A epoxy resin 618 (Wuxi Resin Factory, epoxy value 0.51eq / 100g) 10 grams, dimer acid diglycidyl ester (Nanjing Science and Technology Development Corporation of Forestry Institute, epoxy value 0.29eq / 100g) ) 40 grams, polypropylene glycol diglycidyl ether (Yancheng Hehai Chemical Solvent Co., Ltd., epoxy value 0.28-0.36eq / 100g) 50 grams.
[0028] Part B: Shell No. 90 petroleum asphalt (Shell Company) 150 grams, low molecular weight polyamide 650 curing agent (amine value 200 mg / g) 10 grams, polyetheramine D230 curing agent (Hunsman, molecular weight 230) 30 grams.
[0029] According to the quality of the above formula, bisphenol A epoxy resin 618, dimer acid diglycidyl ester and polypropylene glycol diglycidyl ether were stirred evenly through a colloid mill to obtain part A. According to the quality of the formula, mix Shell No. 90 petroleum asphalt, low-molecular polyamide 650 curing agent and polyetheramine curing agent D230 throu...
Embodiment 2
[0032] formula:
[0033] Part A: 50 g of dimer acid diglycidyl ester (Nanjing Science and Technology Development Corporation of Forestry Institute, epoxy value 0.29eq / 100g), 1,4-butanediol diglycidyl ether (Shanghai Fucane Chemical Co., Ltd.) 50g.
[0034] Part B: Shell No. 70 petroleum asphalt (Shell Company) 50 grams, cardanol phenolic modified amine curing agent (Shanghai Jingtian New Material Co., Ltd., amine value 225mg / g) 50 grams, polyetheramine D230 curing agent (Hens Man company) 50 grams.
[0035] According to the quality of the above formula, dimer acid diglycidyl ester and 1,4-butanediol diglycidyl ether were stirred evenly through a colloid mill to obtain part A. According to the quality of the formula, Shell No. 70 petroleum asphalt, cardanol phenolic modified amine curing agent and polyether amine D230 curing agent were stirred evenly through a colloid mill to obtain part B. After blending Part A and Part B evenly, the viscosity at 25°C was 2100 mPa·s, and cu...
Embodiment 3
[0038] formula:
[0039] Part A: Bisphenol A epoxy resin 618 (Wuxi Resin Factory, epoxy value 0.51eq / 100g) 25 grams, dimer acid diglycidyl ester (Nanjing Science and Technology Development Corporation of Forestry Institute, epoxy value 0.29eq / 100g) ) 25 grams, ethylene glycol diglycidyl ether (99%, Yancheng Hehai Chemical Solvent Co., Ltd.) 50 grams.
[0040] Part B: 300 grams of Shell No. 110 petroleum asphalt (Shell Company), 25 grams of polyetheramine D230 curing agent (Hunsman Company), and 25 grams of m-xylylenediamine curing agent (chemically pure reagent grade).
[0041]According to the quality of the above formula, bisphenol A epoxy resin 618, dimer acid diglycidyl ester and ethylene glycol diglycidyl ether were stirred evenly through a colloid mill to obtain part A. According to the quality of the formula, mix Shell No. 110 petroleum asphalt, polyetheramine D230 curing agent and m-xylylenediamine curing agent through a colloid mill to obtain part B. After blending P...
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