Evaporation-condensation method for preparing superfine metal powder

A technology of ultrafine powder and metal, which is applied in the field of evaporation-condensation preparation of ultrafine metal powder, which can solve the problems of not meeting market demand, low yield of ultrafine powder, low surface activity, etc., and achieves wide application range and high surface activity. Strong, good wetting effect

Inactive Publication Date: 2012-08-01
HANGZHOU HUANA TOWER TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, most mechanical methods have the problem of difficult classification after powder preparation; gas atomization method is currently the main method for preparing high-performance metal and alloy powders, but the production efficiency is low, the yield of ultrafine powder is not high, and the energy consumption is relatively low. Larger, high production cost; Jet milling method and hydrodehydrogenation method are suitable for large-scale industrial production, but have...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] Feed the commercially available raw material copper (16 gauge wire into 1~10mm long) into the crucible of the evaporator through an airtight metal feeder at a feed rate of 3kg / h, and the metal evaporates in the evaporator. The required energy is provided by a high-intensity arc (pressure greater than 10kPa, current greater than 100A) formed between the non-melting electrode (cathode, through cooling water) in the plasma torch on the top of the evaporator and the metal (anode) in the crucible; The working gas is composed of nitrogen and hydrogen, and is continuously fed into the evaporator through the nozzle of the plasma spray gun at a flow rate of 60 lpm (liters per minute). The arc discharge between the cathode and the anode makes the inflowing working gas heated enough High temperature, and then ionized into hot plasma; the raw material in the crucible is melted and evaporated, and interacts with the plasma, the gas carries metal vapor and sprays it into the condenser...

Embodiment 2

[0018] The commercially available diameter is the hemispherical nickel grain of 12mm, is sent in the crucible of evaporator with the feed rate of 2.5 kg / h by airtight metal feeder, and other methods are with embodiment 1, the nickel powder prepared , the nickel content is greater than 99.8%, the hydrogen loss is less than 0.25%, and the particle size is 50-1000 nanometers.

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Abstract

The invention discloses an evaporation-condensation method for preparing superfine metal powder, which comprises the steps that raw materials are fed into a crucible of an evaporator through an airtight metal feeding machine, and the feed speed is 0-10kilogram/hour; metal is evaporated in the evaporator; air containing metal steam is injected into a condensation pipe with the speed of 500-25,000lpm, steam in the condensation pipe is quickly cooled by the condensation pipe through water cooling to form metal powder, the metal powder enters a collector along with the air, and the powder is separated from the air through a set of multi-pore metal filter core device to form pressed powder; and inert gas is reversely blown in to enable the pressed powder to fall and be collected. The superfine powder prepared with the method is good in particle quality, the superfine powder is spherical particles with the particle diameter as 50-2,000 nanometers, and the superfine powder is good in particle size distribution. The method has the advantages of being capable of meeting industrialized scale productivity, low in production cost, small in invest, simple in equipment, easy to control particle size, capable of preparing various types of metal superfine powder, wide in using scope and the like.

Description

technical field [0001] The invention relates to a method for preparing superfine metal powder by evaporation-condensation. Background technique [0002] In the 1960s, someone proposed the concept of ultrafine powder. The particle size of ultrafine powder is generally required to be 0.1~1 micron, and ultrafine powder is also called nanoparticle. By the early 1980s, Japanese scientists began to conduct in-depth research on ultrafine powder, including its characteristics, uses, and manufacturing methods. Due to the efforts of Japanese scientists, the concept of ultrafine powder was finally accepted by people, and it caused scholars and experts from other European and American developed countries, such as the United States, Britain, Germany, France and other countries, to attach great importance to the research of ultrafine powder, resulting in an upsurge . A brand-new science and technology-nanotechnology was born from the research of ultrafine powder. The technology that p...

Claims

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Application Information

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IPC IPC(8): B22F9/12
Inventor 沈树荣孙土金唐素丽沈宏
Owner HANGZHOU HUANA TOWER TECH
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