Method for detecting Danhong injection ethanol precipitation process on line
A Danhong injection and detection method technology, applied in the direction of measuring device, color/spectral characteristic measurement, material analysis through optical means, etc., to achieve the effect of improving quality control level and stabilizing product quality
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[0045] Example 1:
[0046] 1. Install near-infrared online detection device
[0047] See figure 1 , The near-infrared online detection device is composed of the following parts: the near-infrared online detection system includes an alcohol precipitation tank 1, a stirrer 2, a filter 3, a first peristaltic pump 4, a second peristaltic pump 4', and a near-infrared spectrometer 5. , Fiber optic probe 6, flow cell 7, circulation pipeline 8 and alcohol precipitation liquid sampling port 9. The filter 3 is placed in the alcohol precipitation tank 1, and is connected to the first peristaltic pump 4, the flow cell 7 and the alcohol precipitation liquid sampling port 9 through the circulating pipeline 8. The second peristaltic pump 4'is connected to the alcohol precipitation tank 1 and Ethanol solution, the near-infrared spectrometer 5 collects the near-infrared spectrum of the alcohol precipitation liquid in the flow cell 7 through the optical fiber probe 6 online.
[0048] The flow rate ...
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[0064] Example 2:
[0065] According to the method of Example 1, the difference is that the least squares support vector machine (LS-SVM) algorithm is used to establish a quantitative correction model for each quality control index.
[0066] 1. Use the same calibration set sample data as in Example 1.
[0067] Using the same method as in Example 1, the near-infrared spectrum data was preprocessed by the first derivative method (Savitzky-Golay smoothing) and the standard orthogonal transformation algorithm after removing the abnormal spectrum. Use 5445~7500 cm for the soluble solid content model -1 For the band, 5445~6100 cm is used for the models of Danshensu, Protocatechualdehyde, Hydroxysafflor Yellow A and Salvianolic Acid B -1 Band.
[0068] 2. Use Least Squares Support Vector Machine (LS-SVM) algorithm to establish each quality control index model
[0069] After obtaining the characteristic spectrum information of the alcohol precipitation liquid, the least squares support vecto...
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