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Method for preparing zinc oxide nanoshuttle

A technology of zinc oxide nano and zinc nitrate, applied in the direction of zinc oxide/zinc hydroxide, nanotechnology, etc., can solve the problems of high cost, complex equipment, high reaction temperature, etc., and achieve pure crystallization, low reaction temperature and good repeatability Effect

Inactive Publication Date: 2012-09-12
HARBIN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The invention solves the technical problems of complex equipment, high cost and high reaction temperature in the existing preparation method for preparing zinc oxide micro-nano structure, and provides a method for preparing zinc oxide nano-shuttle

Method used

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  • Method for preparing zinc oxide nanoshuttle
  • Method for preparing zinc oxide nanoshuttle
  • Method for preparing zinc oxide nanoshuttle

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specific Embodiment approach 1

[0014] Specific embodiment one: the method for preparing zinc oxide nano-shuttle in the present embodiment is as follows:

[0015] Step 1, the Zn(NO of 0.005mol 3 ) 2 ·6H 2 The hexamethylenetetramine of 0 and 0.005mol is added into the distilled water of 25ml respectively and stirred and dissolved, and zinc nitrate solution and hexamethylenetetramine solution are obtained;

[0016] Step 2, slowly drop the zinc nitrate solution into the hexamethylenetetramine solution, stir while adding dropwise, then add dropwise 10ml of ammonia solution with a mass concentration of 25%, and then seal the obtained mixed solution;

[0017] Step 3, stirring the mixed solution on a magnetic stirrer at a speed of 300 rpm for 3 to 5 minutes to obtain a transparent and clear solution;

[0018] Step 4. Pour the clarified solution into a stainless steel reactor lined with polytetrafluoroethylene, then place the reactor in a vacuum oven at 130°C, keep it warm for 12-18 hours, then take out the react...

specific Embodiment approach 2

[0020] Embodiment 2: This embodiment differs from Embodiment 1 in that the holding time described in step 4 is 12 hours. Others are the same as in the first embodiment.

specific Embodiment approach 3

[0021] Embodiment 3: This embodiment is different from Embodiment 1 in that the holding time in step 4 is 13 hours. Others are the same as in the first embodiment.

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Abstract

The invention relates to a method for preparing zinc oxide nanoshuttle, and provides a method for preparing a ZnO micro nano material with new appearance by a simple low-temperature hydro-thermal synthesis technology. The method comprises the following steps of: dripping a zinc nitrate solution into a hexamethylenetetramine solution slowly, dripping an ammonia water, and stirring; pouring the mixture into a reaction kettle, drying and diluting; and centrifuging a diluent to obtain a precipitate, drying the precipitate, and grinding to obtain the zinc oxide nanoshuttle. According to the zinc oxide nanoshuttle, the average value of the diameter of an intermediate section of a shuttle body is 500 nanometers, and the average length of the shuttle body is 1 to 2 micrometers. The zinc oxide nanoshuttle is pure in crystallization, and uniform in appearance and in size, and can be used for the fields of photochemical catalysis, gas sensitive sensors, moisture-sensitive sensors, photoelectronic devices, piezoresistors and the like.

Description

technical field [0001] The invention relates to a method for preparing zinc oxide nano shuttle. Background technique [0002] The structure and morphology of micro-nano materials have a great influence on the properties and applications of micro-nano materials. The preparation of micro-nano materials with specific structures has important academic significance and application value for the development of new fields of properties of micro-nano materials. Among numerous micro-nano materials, the micro-nano structure of ZnO has received extensive attention. Zinc oxide with micro-nano structure has attracted much attention due to its large specific surface area and good magnetic, optical, and electrical properties. It is expected to be used in many fields such as photocatalysis, gas sensors, humidity sensors, piezoresistors, and transparent electrodes. with broadly application foreground. [0003] At present, the preparation methods of ZnO micro-nanostructure mainly include c...

Claims

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Application Information

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IPC IPC(8): C01G9/02B82Y40/00
Inventor 岳红彦王丽萍张建交冯义成
Owner HARBIN UNIV OF SCI & TECH
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