Extracting method and new usage of chalcone in Coreopsis grandiflora
A technology of coreopsis and mesochalcone, which is applied in the fields of chemistry and agriculture, and can solve problems such as no biological activity
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[0019] Example 1 Extraction of compound 2',4',4-trihydroxy-3',3-dimethoxychalcone
[0020] 5000g coarse powder of dried flowers of Coreopsis grandiflora was soaked and extracted with 95% ethanol for 3 times for 3d, 5d and 7d. After the extracts were combined, the solvent was recovered under reduced pressure to obtain 1140 g of 95% ethanol extract. After 1140 g of 95% ethanol extract was added to 10 times the amount of distilled water to suspend, ethyl acetate was added to extract 4 times. After recovering the solvent, 172 g of ethyl acetate extract was obtained. Take 40g of ethyl acetate extract and chromatograph on silica gel column, and then use 2:1 and 1:1 volume ratio of petroleum ether + chloroform, pure chloroform, 100:1~1:5 volume ratio of chloroform + methanol and pure methanol. Gradient elution gave 2',4',4-trihydroxy-3',3-dimethoxychalcone as orange crystals. The spectral data of the structure identification of the above isolated compound 2',4',4-trihydroxy-3',3-d...
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[0023] Experimental example 2 2',4',4-trihydroxy-3',3-dimethoxychalcone and its herbicidal activity in each extraction stage
[0024] 1) Experimental materials
[0025] Lettuce, amaranth, cucumber, wheat
[0026] 2) Experimental method
[0027] Agar method: After soaking the recipient plant seeds in a 0.2% sodium hypochlorite solution for 15 minutes, rinse them with tap water several times and soak them under running water to absorb water for about 3~5 hours, then wash them several times with distilled water and place them evenly on a square plate with a lid On the absorbent paper inside, drip distilled water until the seeds do not float, shading and place them in a fully intelligent artificial climate box (HP1000GS-B, Wuhan Ruihua Instrument and Equipment Co., Ltd.) to germinate until the radicle (or seed root) reaches 3 When ~5 mm, transplant to 0.5% agar gel (prepared 100 mL in advance and evenly dispensed into 3 small beakers) mixed with extracts of various stages. The extract...
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