Method for coproducing egg yolk lecithin, cephalin, yolk oil and low-denatured protein flour
A low-denatured protein powder and egg yolk lecithin technology, which is applied in the preparation method of peptides, fat oil/fat production, edible phospholipid composition, etc., can solve the problem of organic solvents not meeting environmental protection requirements, large consumption of organic solvents, and food safety hazards and other problems, to achieve the effect of shortening the production cycle, short separation cycle and speeding up the dissolution rate
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Embodiment 1
[0033] 100.0 kg of fresh eggs were sorted and washed, then sterilized (soaked in boiling water at 95-100°C for 5-7 s), air-dried, and separated from the egg white and yolk by egg white and egg yolk separation equipment to obtain 28.0 kg egg yolk. Add 28 L of water to the egg yolk liquid to dilute and stir evenly, then add the egg yolk dilution into the extraction tank, then add 56 L of 80% ethanol solution, extract at 20 KHz, 45 °C for 10 min, pulse interval After extraction for 1 s, the extract was filtered, and the filtrate was left standing overnight at room temperature to discard the precipitate to obtain egg yolk neutral fat extract (containing egg yolk phospholipids), which was concentrated under reduced pressure at 45 °C to a thick paste, recovered Solvent, the obtained thick paste was vacuum-dried at 55 °C to obtain 4.1 kg of light yellow egg yolk lecithin crude extract; collected ethanol insoluble matter, evaporated the residual ethanol solvent under reduced pressure,...
Embodiment 2
[0038] 100.0 kg of fresh eggs were sorted and washed, then sterilized (soaked in boiling water at 95-100°C for 5-7 s), air-dried, and separated from the egg white and yolk by egg white and egg yolk separation equipment to obtain 28.0 kg egg yolk. Add 28 L of water to the obtained egg yolk liquid to dilute and stir evenly, then add the egg yolk dilution into the extraction tank, then add 504 L of ethanol solution with a mass fraction of 95%, and extract 5 times at 80 KHz and 60 °C, each time 60 min, pulse interval 5 s, after extraction, the extract was filtered, and the filtrate was left standing overnight at room temperature to discard the precipitate to obtain egg yolk neutral fat extract (containing egg yolk phospholipid), which was concentrated under reduced pressure at 50 °C to Thick paste, recover the solvent, vacuum-dry the obtained thick paste at 65 °C to obtain 8.1 kg of light yellow egg yolk lecithin crude extract; collect ethanol insoluble matter, evaporate the resid...
Embodiment 3
[0043] 100.0 kg of fresh eggs were sorted and washed, then sterilized (soaked in boiling water at 95-100°C for 5-7 s), air-dried, and separated from the egg white and yolk by egg white and egg yolk separation equipment to obtain 28.0 kg egg yolk. Add 56 L of water to the obtained egg yolk liquid for dilution and stir evenly, then add the egg yolk dilution into an ultrasonic extraction tank, then add 126 L of 90% ethanol solution, and extract twice at 40 KHz and 55 °C, each time 30 min, with a pulse interval of 2 s. After extraction, the extract was filtered, and the filtrate was left at room temperature overnight to discard the precipitate to obtain egg yolk neutral fat extract (containing egg yolk phospholipids), which was concentrated under reduced pressure at 50 °C to Thick paste, recover the solvent, vacuum-dry the obtained thick paste at 55 °C to obtain 7.5 kg of light yellow egg yolk lecithin crude extract; collect ethanol insoluble matter, evaporate the residual ethanol...
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