Preparation method for active mixed extract of tea tree oil meal as well as extract and application of extract
A technology of mixed extraction and tea tree oil, applied in botany equipment and methods, applications, food science, etc., can solve the problems of low utilization rate, waste of resources, and no research and application reports, and achieve the goal of overcoming limitations and waste of resources Effect
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Embodiment 1
[0037] Embodiment 1 The preparation of tea tree oil meal extract
[0038] The tea tree oil meal comes from a tea tree oil manufacturer in Zhaoqing City, Guangdong Province (tea tree oil meal produced by oil extraction from other manufacturers can also be used, and the present invention is not limited thereto), and other reagents are commercially available conventional products. For the convenience of illustration, the tea tree oil meal used in this example comes from the Nanshan tea seed kernel for preparing tea tree oil.
[0039]After drying the tea tree oil meal, grind it into a powder with a pulverizer, pass through a 100-mesh sieve, and separate quickly to obtain a tea tree oil meal fine powder; add 3500 mL of pure water to 500 g of the tea tree oil meal fine powder, and extract the tea tree overnight at 85°C Oil meal fine powder, filter or centrifuge to obtain 800 mL of filtrate, add 800 mL of petroleum ether to the filtrate, extract 360 mL of tea tree oil meal extract a...
Embodiment 2
[0046] Example 2 Preparation of tea tree oil meal extract
[0047] The tea tree oil meal comes from a tea tree oil manufacturer in Zhaoqing City, Guangdong Province (tea tree oil meal produced by oil extraction from other manufacturers can also be used, which does not limit the present invention, and the type of tea tree is not limited), and other reagents are commercially available conventional products. After drying the tea tree oil meal, grind it into a powder with a pulverizer, pass through a 50-mesh sieve, and separate quickly to obtain a tea tree oil meal fine powder; add 3000 mL of pure water to 500 g of the tea tree oil meal fine powder, and extract the tea tree overnight at 90°C Oil meal fine powder. Filtrate or centrifuge to obtain 450 mL of filtrate, add 900 mL of petroleum ether to the filtrate, extract for 24 hours, obtain 300 mL of tea tree oil meal extract, obtain 140 mL of concentrated extract through rotary concentration, and dry the concentrated extract at ...
Embodiment 3
[0049] Example 3 Preparation of tea tree oil meal extract
[0050] The tea tree oil meal comes from a tea tree oil manufacturer in Zhaoqing City, Guangdong Province (tea tree oil meal produced by oil extraction from other manufacturers can also be used, and the present invention is not limited thereto), and other reagents are commercially available conventional products. After drying the tea tree oil meal, grind it into a powder with a pulverizer, pass through a 30-mesh sieve, and separate quickly to obtain a tea tree oil meal fine powder; add 2500 mL of pure water to 500 g of the tea tree oil meal fine powder, and extract the tea tree overnight at 95°C Oil meal fine powder. Filtrate or centrifuge to obtain 680 mL of filtrate, add 1800 mL of petroleum ether to the filtrate, and extract for 24 hours to obtain 340 mL of tea tree oil meal extract, which is concentrated by rotation to obtain 160 mL of concentrated extract, and the concentrated extract is dried at a constant temp...
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