Fibre cloth reinforced modified polyarylene sulfide sulfone composite material and preparation method thereof
A polyarylene sulfide sulfone and composite material technology, which is applied in chemical instruments and methods, synthetic resin layered products, lamination, etc., can solve the problems of high viscosity, difficult to achieve good impregnation of fiber cloth by resin matrix, etc. Low equipment requirements, operability, and environmental friendliness
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Embodiment 1
[0029] (1) Dry 100 parts of polyarylene sulfide sulfone resin, 10 parts of polyphenylene sulfide resin, 5 parts of zinc oxide and 5 parts of DTBHQ in an oven at a temperature of 100°C for 8 hours, and mechanically blend in a high mixer;
[0030] (2) Melt, blend, extrude and granulate the above blended materials with a twin-screw extruder at a temperature of 340°C, and dry them in an oven at a temperature of 100°C for 8 hours; pass the obtained blend pellets through a single-screw extruder at a temperature Melt extrusion at 340°C, and the blend film was obtained by three-roll calender shaping;
[0031] (3) The above-mentioned diaphragm and fiber cloth are laminated alternately in the order of A-layer / B-layer unit structure to form a fiber cloth-reinforced modified polyarylene sulfide sulfone composite layer: A layer is the above-mentioned polyarylene sulfide sulfone blend film, B layer is carbon fiber cloth (40 parts);
[0032] (4) The above-mentioned composite layer was hot-p...
Embodiment 2
[0037] (1) Dry 100 parts of polyarylene sulfide sulfone resin, 40 parts of polyphenylene sulfide resin, 5 parts of zinc acetate and 5 parts of BHT in a blast oven at a temperature of 110 ° C for 7 hours, and mechanically blend in a high-speed mixer;
[0038] (2) Melt, blend, extrude and granulate the above-mentioned blended materials with a twin-screw extruder at a temperature of 320°C, and dry them in a blast oven at a temperature of 110°C for 7 hours; pass the obtained blend pellets through a single-screw extruder Melt and extrude at a temperature of 320°C, and obtain a blend film after shaping by a three-roll calender;
[0039] (3) The above-mentioned diaphragm and fiber cloth are laminated alternately in the order of A-layer / B-layer unit structure to form a fiber cloth-reinforced modified polyarylene sulfide sulfone composite layer: A layer is the above-mentioned polyarylene sulfide sulfone blend Material diaphragm, B layer is quartz fiber cloth (200 parts);
[0040] (4) ...
Embodiment 3
[0045] (1) Dry 100 parts of polyarylene sulfide sulfone resin, 60 parts of polyphenylene sulfide resin and 5 parts of DTBHQ in a blast oven at a temperature of 120 ° C for 6 hours, and mechanically blend in a high-speed mixer;
[0046] (2) Melt, blend, extrude and granulate the above-mentioned blended materials with a twin-screw extruder at a temperature of 310°C, and dry them in a blast oven at a temperature of 120°C for 6 hours; pass the obtained blend pellets through a single-screw extruder Melt and extrude at a temperature of 310°C, and obtain a blend film after being shaped by a three-roll calender;
[0047] (3) The above-mentioned diaphragm and fiber cloth are laminated alternately in the order of A-layer / B-layer unit structure to form a fiber cloth-reinforced modified polyarylene sulfide sulfone composite layer: A layer is the above-mentioned polyarylene sulfide sulfone blend material film, layer B is aramid fiber cloth (300 parts);
[0048] (4) The above-mentioned com...
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