Sensing film ion selective electrode prepared by film dropping method

A technology of ion-selective electrodes and sensing membranes, applied in the direction of material analysis, measuring devices, and instruments through electromagnetic means, can solve problems such as high assembly process requirements, affecting electrode performance, and membrane deformation and arching, so as to improve economic benefits , Electrode performance is reliable and stable, and the effect of saving film making time

Active Publication Date: 2013-02-27
SHANGHAI HUIZHONG MEDICAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In this method, the membrane solution is directly dropped into the electrode chamber. Generally, the material of the electrode chamber is plexiglass. Most or all of the solute of the membrane solution is tetrahydrofuran, which can corrode all plastic products. Some additives in the plexiglass material in the electrode cavity will Dissolving into the membrane liquid, such as silicon-containing fillers, will destroy the adsorption of ions by the sensing membrane and affect the performance of the sensing membrane
However, in the structure of the inner cavity of the electrode, the place where the membrane solution is dropped is a conical shape with a hole at the bottom. The membrane formed by the first layer of dripping is just in direct contact with the calibration solution or test solution, which will affect the performance of the electrode.
However, the film loading method generally prefabricates the film, and then presses the film assembly into the electrode body cavity. This method has high requirements for the assembly process, and the film must be pressed in place. If it is too loose, the solution on the inner and outer surfaces of the film will short-circuit. If it is too tight, it will cause the membrane to deform and arch and cannot contact the sample solution. If it is too loose or too tight, the electrode will be scrapped. The success rate of assembly is not as high as that of the drop film method.

Method used

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  • Sensing film ion selective electrode prepared by film dropping method
  • Sensing film ion selective electrode prepared by film dropping method
  • Sensing film ion selective electrode prepared by film dropping method

Examples

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Embodiment Construction

[0028] Example 1~6, such as Figure 1~4 As shown, the preparation of the drop film method induction membrane ion selective electrode:

[0029] 1. Membrane dripping: drip the prepared ionic membrane liquid into the PVC ring 6 under the condition of the fume hood. After the solvent in the previous film liquid is evaporated to dryness, another layer of film liquid is dropped, and the film is dripped repeatedly in this way to form a K, Cl, Ca or other ion-sensitive film 7 with the same thickness as the PVC ring 6 .

[0030] 2. Make the electrode core: Weld the contact 1 with the Ag / AgCl wire 2, and then bond the contact 1 with the mounting head 3 with epoxy resin, and insert the O-ring a4 into the groove of the mounting head 3.

[0031] 3. Electrode chamber: Put the PVC ring 6 that has been filmed into the inner cavity of the electrode body 8 (the surface of the last layer of film faces down), then put the pressure ring 5 into the electrode body 8, and press the pressure ring 5...

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Abstract

The invention relates to a blood gas electrolyte analyzer, in particular to a sensing film ion selective electrode in the blood gas electrolyte analyzer. The sensing film ion selective electrode comprises an electrode chamber and an electrode core, wherein the electrode core comprises a contact, a Ag / AgCl wire, an installation head and an O-shaped ring a; the contact is connected with the Ag / AgCl wire in a welding manner and is adhered to the installation head by epoxy resin; the O-shaped ring a is sleeved in a groove of the installation head; the electrode chamber comprises a pressure ring, a PVC (Poly Vinyl Chloride) ring, a sensing film, an electrode body and an O-shaped ring c; the sensing film is prepared by dropping prepared corresponding film liquid into the PVC ring; and when the sensing film ion selective electrode is assembled, the PVC ring in which the sensing film is formed is placed into an electrode body chamber in the direction that the side of the final layer of dropped film is downwards, then the pressure ring is placed in the electrode body, the pressure ring is pressed to a designated position to fix the sensing film, the O-shaped ring c is sleeved in a groove at the lateral surface of the electrode body, electrode inner liquid is filled in the electrode chamber and the electrode core is screwed into the electrode body chamber so as to form the sensing film ion selective electrode prepared by a film dropping method.

Description

technical field [0001] The invention relates to a blood gas electrolyte analyzer, in particular to a sensing membrane ion selective electrode in the blood gas electrolyte analyzer. Background technique [0002] Electrolytes play an important role in maintaining the balance of the internal environment and normal physiological functions of the human body. Plasma sodium accounts for 92% of total plasma ions and 90% of osmotic pressure, so plasma sodium plays a decisive role in osmotic pressure and is regulated by hypothalamus, posterior pituitary and kidney. Potassium accounts for 98% of the total in cells, and it is of great significance in maintaining the osmotic pressure of intracellular fluid, capacity and substance metabolism, acid-base balance, stress of neuromuscular cell membranes, and maintaining the normal function of myocardium. Cl is the main anion in the extracellular fluid, and Ca ions are the main constituents of bones, which regulate muscle contraction and bloo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N27/333
Inventor 蒋丽敏王庆厚冬连红王娜张凯峰
Owner SHANGHAI HUIZHONG MEDICAL TECH
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