Celastrus angulatus and cnidium lactone compounded pesticide and preparation method thereof
A technology of osthole and fenugreek, which is applied in the directions of pesticides, botanical equipment and methods, biocides, etc., to achieve the effects of improving the effect, reducing the amount of pesticides, and reducing the cost of prevention and control.
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Embodiment 1
[0035] Embodiment 1: According to the raw materials corresponding to Embodiment 1 in Table 1 and their weight ratios, a sufficient amount of bamboo vinegar or wood vinegar was left to stand for 5 to 8 months and then filtered to make mother liquor, and then 0.1 part of bitter bark Rattan, 0.1 part of osthole and 0.5 part of antioxidant are added to 5 parts of organic solvents for dissolving, and the colloid is ground and mixed evenly to make the oil phase, and then a small amount of bamboo (wood) vinegar is added to 5 parts of emulsifier, and after stirring As the water phase, mix the water phase and the oil phase through a colloid mill, then add a small amount of bamboo vinegar or wood vinegar to the remaining other additives according to their respective weight parts, and mix this mixture with the water phase and oil phase mixture Together, grind and mix evenly in a colloid mill, and finally add the remaining bamboo (wood) vinegar to make the total amount of bamboo (wood) vin...
Embodiment 2~9
[0036] The rest of Examples 2 to 9 were all prepared in the same way as Example 1 according to the raw materials and their weight ratios of the corresponding examples in Table 1, and Example 4 was preferred.
[0037] Table 1 Nine Examples of Raw Material Types and Their Weight Ratio Values
[0038]
[0039] The indoor virulence determination experiment relevant to the application and the situation of the field control effect test including five examples are made an introduction below:
[0040] 1. Indoor toxicity test
[0041] 1.1 Materials and methods
[0042] 1.1.1 Test insects
[0043] Pear gall midges were collected from the field, and healthy 2nd instar larvae of the same size were selected in the laboratory as test insects.
[0044] 1.1.2 Drugs to be tested
[0045] 6% picroderm, Xinxiang Dongfeng Chemical Co., Ltd.; 20% osthole, Xi'an Tianben Bioengineering Co., Ltd. The test medicaments paretin (A) and osthole (B) were dissolved with acetone and diluted to 1000 mg...
example 1
[0054] The preparation method of example one compound insecticide is:
[0055] (1) Let the bamboo (wood) vinegar solution stand for 5 to 8 months, filter it, and collect it as mother liquor.
[0056] (2) According to the proportion, bitter bark vine, osthole and tocopherol are added to ethanol and ethyl acetate as the solvent to dissolve, and the oil phase is obtained by mixing evenly through the colloid mill; the colloid mill does not make special requirements, and can reach The effect of mixing is even.
[0057] (3) Add an appropriate amount of bamboo (wood) vinegar obtained in step (1) into the polyoxyethylene sorbitan fatty acid ester and castor oil polyoxyethylene ether as emulsifiers, stir and dissolve, and obtain an aqueous phase.
[0058] (4) Add the water phase to the oil phase, and mix evenly through a colloid mill.
[0059] (5) Add an appropriate amount of bamboo (wood) vinegar obtained in step (1) to the other additives, stir and dissolve, then add the mixture ob...
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