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Cement slurry and preparation method and application thereof

A cementing cement slurry and cement slurry technology, which is applied in chemical instruments and methods, earthwork drilling, wellbore/well components, etc., can solve the problems of corrosive medium corrosion, poor stability of cement slurry system, and slow development of cement stone strength, etc. problems, to achieve the effects of enhancing compactness and structural strength, improving compactness and structural strength, and preventing formation fluid from entering the annular space

Active Publication Date: 2013-07-31
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Due to the incorporation of a large amount of external admixtures in low-density cement slurry, the density of the cement slurry is reduced, the stability of the cement slurry system is poor, and the system is delaminated and segregated; the water loss of the cement slurry is difficult to control; the rheological properties of the cement slurry are poor and pumping is difficult; Slow strength development, low strength, high permeability of cement slurry, easy to cause corrosion of corrosive media
[0005] At present, the ultra-low density lightening materials that can be provided in China cannot meet the requirements of ultra-low density cement slurry in terms of strength, activity, and slurry mixing performance; it is possible to use foam cement slurry to achieve ultra-low density cement slurry However, due to the influence of downhole temperature and pressure, the conventional foam cement slurry has a large difference between the actual density and the ground density, and the strength is low at low temperature. Due to the shortcomings of comprehensive performance requirements, it is difficult for a single ultra-low density foam cement slurry to meet the requirements of high strength, low permeability and downhole cement slurry density, so the low density high strength cement slurry system is studied on the basis of existing technologies

Method used

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  • Cement slurry and preparation method and application thereof
  • Cement slurry and preparation method and application thereof
  • Cement slurry and preparation method and application thereof

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Experimental program
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Effect test

Embodiment 3

[0070] The product of the embodiment of the present invention is prepared according to the following method (example with the formula of Example 3):

[0071] Preparation method of low-density high-strength cement slurry for low-pressure and easy-to-leak multi-oil layer cementing:

[0072] 1. Calculate the weight of cement and water according to the required water-cement ratio (water-cement ratio is 0.5);

[0073] 2. Weigh 70 parts of cement on a platform scale or balance, measure 35 parts of corresponding water with a graduated cylinder, start the mixer, and adjust the rotation speed to 4000r / min;

[0074] 3. Take 25 parts of alleviating agent with standard balance, put into the water of step 2, adjust the number of revolutions to be 4000r / min;

[0075] 4. Weigh 4 parts of the enhancer with a standard balance, put them into the water in step 3, and adjust the number of revolutions to 4000r / min;

[0076] 5. Use a standard balance to weigh 0.5 part of fluid loss reducer, ...

Embodiment 1

[0082] The density is 1.44g / cm 3 Low-density, high-strength cement slurry for low-pressure, leaky multi-oil interval cementing:

[0083] The low-density and high-strength cement slurry for cementing the low-pressure, leaky and multi-oil intervals is as follows in parts by weight:

[0084] 75 parts of cement, the cement is Jiahua G grade cement;

[0085] 30 parts of lightening agent, the lightening agent produced by Xi'an Changqing Technology Co., Ltd. is hollow microbeads 58% SiO 2 , 35%Al 2 o 3 , 3.4%Fe 2 o 3 , 2.0%CaO, 1.6%MgO; the particle size is 56-360μm, and the density is 0.80g / cm 3 ;

[0086] 6 parts of reinforcing agent, the reinforcing agent is the micro-gelled material produced by Xi'an Changqing Technology Co., Ltd., and 100 parts by weight contain the parts by weight of the following chemical components: 92% SiO 2 , 2.7%Al 2 o 3 , 0.80%Fe 2 o 3 , 2.54%CaO, 0.36%MgO, 1.6%P 2 o 5 The particle size distribution is 0.1μm: 15%, 0.1~0.5μm: 48%; 0.5~1.0μm: ...

Embodiment 2

[0092] The density is 1.25g / cm 3 Low-density, high-strength cement slurry for low-pressure, leaky multi-oil interval cementing:

[0093] 65 parts of cement, the cement is Jiahua G grade cement;

[0094] 20 parts of lightening agent, lightening agent is hollow microsphere 58%SiO 2 , 35%Al 2 o 3 , 3.4%Fe 2 o 3 , 2.0%CaO, 1.6%MgO; the particle size is 56-360μm, and the density is 0.80g / cm 3 ;

[0095] 3 parts of reinforcing agent, the reinforcing agent is the fine gelled material produced by Xi'an Changqing Science and Technology Co., Ltd., contains the weight part of following chemical composition in its 100 parts by weight: 92% SiO 2 , 2.7%Al 2 o 3 , 0.80%Fe 2 o 3 , 2.54%CaO, 0.36%MgO, 1.6%P 2 o 5 The particle size distribution is 0.1μm: 15%, 0.1~0.5μm: 48%; 0.5~1.0μm: 20%; 1.0~3.0μm: 10%; 3.0~10.0μm: 5%; 10.0~200μm: 7%;

[0096] 0.3 parts of fluid loss reducer, the fluid loss reducer is a mixture of sulfonated polystyrene and sulfonated polymethylstyrene in a wei...

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Abstract

The present invention relates to a cement slurry and a preparation method and application thereof, wherein the cement slurry includes the following components in parts by weight of 65 to 75 parts of cement, 20 to 30 parts of reducing agent, 3 to 6 parts of reinforcing agent, 0.3 to 1 parts of filtrate reducer, 2 to 4 parts of early strength agent, 0.6 to 1.0 parts of retarder, 60 to 80 parts of water, wherein the reducing agent is the hollow microsphere containing main components of silicon dioxide, aluminum oxide, lime, magnesium oxide and ferric oxide, with particle size of between 56 and 360Mum and density of 0.80g / cm3; the reinforcing agent powder has specific surface area of between 15 and 20m2 / g and particle size range of between 0.1 and 200 Mum with particle size distribution of 0.1 Mum: 15%; 0.1-0.5 Mum: 45-50%; 0.5-1.0 Mum: 10-20%; 1.0-3.0 Mum: 5-10%; 3.0-10.0 Mum: 5%; 10.0-200 Mum: 7-12%. The cement slurry can adequate return the slurry to the top position and improve the cementing quality of low-pressure leaky well section. The cement slurry has small initial consistency, which is beneficial for on-the-site mixing, flow resistance reducing, and the high-temperature performance is table and the thickening time is adjustable.

Description

technical field [0001] The invention relates to a well cementing cement slurry, its preparation method and application. Background technique [0002] At present, my country's undeveloped reserves total 3.5 billion tons, 70% of which are low-pressure reservoirs, which are prone to leakage during drilling. In the process of underbalanced drilling, the proportion of mud is below 1.0, and the proportion of cement slurry is required to be 0.95-1.10g / cm 3 , some low-permeability (0.025-15.6md), low-porosity, low-abundance, and low-yield oil and gas reservoirs have multiple pressure layers. In order to improve the success rate of exploration, prevent leakage and formation pollution, reduce costs, and achieve one-time sealing , requires the use of ultra-low density cement slurry for effective isolation. Cementing in low-pressure and leaky formations is a difficult problem for drilling technology. Due to the low pressure bearing capacity and high cementing slurry density in low-pres...

Claims

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Application Information

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IPC IPC(8): C09K8/467C09K8/473C09K8/487E21B33/13
Inventor 赵巍李宪文巨满成吴学升李波高云文王勇茗徐自强
Owner PETROCHINA CO LTD
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