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Technology process for producing biodiesel and key preparation device

A biodiesel and preparation device technology, applied in the chemical industry, can solve the problems of high equipment requirements, high investment and operation costs, high reaction pressure, high temperature, etc., and achieve low investment and operation costs, wide application range of raw materials, and low equipment requirements Effect

Inactive Publication Date: 2013-08-14
阳谷县凯歌新能源生物科技有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is: to overcome existing biodiesel production technology, need catalyst, serious environmental pollution, high reaction pressure, temperature, high requirement to equipment, high investment and operation cost, high requirement to raw material, poor selectivity, reaction Shortcomings such as long time, high energy consumption, and low yield provide a method that does not require the use of catalysts, has no environmental pollution, low reaction pressure and reaction temperature, low energy consumption, low investment and operating costs, and a wide range of raw materials. Process technology and key preparation equipment for biodiesel production with high yield

Method used

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  • Technology process for producing biodiesel and key preparation device
  • Technology process for producing biodiesel and key preparation device
  • Technology process for producing biodiesel and key preparation device

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Embodiment Construction

[0024] Such as figure 1 As shown, the process technology for producing biodiesel is mainly completed sequentially according to the following steps:

[0025] The first step is to add the raw oil and softened water into the hydrolysis reaction tower through the metering pump, and carry out the hydrolysis reaction under certain conditions to generate fatty acid and glycerin. The molar ratio of water to oil is 4-5:1, and the reaction temperature is 170- 190°C, reaction pressure 1.2-1.6Mpa, reaction time 2-3 hours;

[0026] The second step is to separate the fatty acid from the glycerol-water mixture through a hydrocyclone, the fatty acid enters the esterification reaction tower, and the glycerin-water mixture is concentrated to form glycerol;

[0027] The third step is to add a certain amount of fatty acid to the esterification reaction tower, then feed gaseous methanol into the esterification reaction tower, and the fatty acid and methanol carry out esterification reaction under...

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Abstract

The invention discloses a technology process for producing biodiesel and a key preparation device. The technology process mainly comprises the following steps of: carrying out hydrolysis reaction on raw material oil and softened water so as to generate fatty acid; carrying out esterification reaction on the fatty acid separated by a cyclone hydraulic separator and methyl alcohol under a certain condition, thereby preparing coarse fatty acid methyl ester, and separating; and distilling the coarse fatty acid methyl ester by a distilling tower, and separating, thereby obtaining fatty acid methyl ester-biodiesel. The key preparation device for achieving the technology process is a reaction tower which mainly comprises a tower body, a heavy separator, a baffle plate, an overhauling port, a distributor, a gas phase methyl alcohol inlet, a material outlet, a water outlet, a heat conduction oil inlet, a heat conduction oil outlet, a heat conduction oil jacket, a material inlet, a water inlet, a safety valve, a temperature meter, a pressure meter and a gas phase methyl alcohol outlet. The technology process for producing biodiesel and the key preparation device have the characteristics of no need of catalysts, no environmental pollution, low reaction pressure and reaction temperature, less energy consumption, low investment and running costs, wide raw material application range, high yield and the like.

Description

Technical field [0001] The invention belongs to the technical field of chemical industry, and specifically relates to a technical process and a key preparation device for producing biodiesel. Background technique [0002] With the increasingly tense international energy situation, especially under the background of the country's vigorous promotion of energy conservation and emission reduction, biodiesel, as a renewable new energy source, can be used as a substitute for petroleum fuels, and has gradually attracted widespread attention from the whole society. "Biodiesel The biggest feature of "diesel" is its renewable nature, and the resource will never be exhausted. Biodiesel can be produced from vegetable oil and animal oil, but at present, fatty acids, swill oil, urban gutter oil, and refining waste are mostly used as raw materials for production. Waste edible oil refers to the non-edible animal and vegetable oil produced in the production and operation process of catering...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11C3/00C11B3/12C11B3/00C11C1/04C10L1/02
CPCY02E50/13Y02E50/10
Inventor 罗凯李京楠仇涛惠庆达
Owner 阳谷县凯歌新能源生物科技有限公司
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