Preparation method of high alkaline shale sintered brick
A high-alkali shale and sintered brick technology, which is applied in the field of building wall materials, can solve the problems of frost back, increased surface area, hollow bulge, etc., and achieves the effects of good anti-frost effect, improved service life, simple and stable process
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Embodiment 1
[0017] K first 2 O content is 1% and Na 2 O2% high-alkali shale is crushed to 0.125mm-0.25mm, add coal powder of 0.125mm-0.25mm and stir in hot water at 60°C for 10 minutes, enter the aging warehouse for 48 hours, and extrude in the extruder Forming, the green body obtained after forming is in the waste heat environment provided by the sintering kiln (the CO containing CO provided by the kiln exhaust gas of the conventional process 2 or CO 2 with SO 3 The high-temperature gas, the same below), is cured for 20 hours at a humidity of 100% and a temperature of 300°C for 20 hours, and then after 8 hours in an environment with a humidity of 20% and a temperature of 250°C, it is cooled to room temperature and calcined in a conventional tunnel kiln. The calcination temperature is 1080-1200°C (30-50°C higher than the existing calcination temperature), and the sintering time is 7-13h (1-3h longer than the existing sintering time), which can meet the requirements of slight frost retu...
Embodiment 2
[0019] K first 2 O content is 3% and Na 2 O2% high-alkali shale is crushed to 0.125mm-0.25mm, add coal powder of 0.125mm-0.25mm and stir in hot water at 80°C for 10 minutes, enter the aging warehouse for 20 hours, and extrude in the extruder Forming, the green body obtained after forming is cured in the waste heat environment provided by the sintering kiln with a humidity of 80% and a temperature of 200°C for 48 hours, and then in an environment with a humidity of 0% and a temperature of 250°C for 9 hours, and then cooled to room temperature. Carry out calcination in a conventional wheel kiln, the calcination temperature is 1080-1200°C (30-50°C higher than the existing calcination temperature), and the sintering time is 7-13h (1-3h longer than the existing sintering time), which can be satisfied Sintered shale bricks required for slight frost return in GB T2542.
Embodiment 3
[0021] K first 2 O content is 2.5% and Na 2 O1% high-alkali shale is crushed to 0.125mm-0.25mm, add coal powder of 0.125mm-0.25mm and stir in hot water at 80°C for 10 minutes, enter the aging warehouse for 30 hours, and extrude in the extruder Forming, the green body obtained after forming is cured in the waste heat environment provided by the sintering kiln with a humidity of 90% and a temperature of 250°C for 36 hours, in an environment with a humidity of 10% and a temperature of 250°C for 10 hours, and then cooled to room temperature. Calcination is carried out in a conventional wheel kiln, the calcination temperature is 1080-1200°C (30-50°C higher than the existing calcination temperature), and the sintering time is 7-13h (1-3h longer than the existing sintering time), which can meet the GB Sintered shale bricks required for slight frost return in T2542.
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