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Multifunctional experiment device and method for deposition of zinc alloy coating

An experimental device and multi-functional technology, applied in metal material coating process, coating, sputtering plating, etc., can solve the problems of application limitations, long production cycle, missing plating, etc., and achieve good automatic control performance and short preparation cycle Effect of shortening and saving workshop space

Active Publication Date: 2013-11-20
北京钢研新冶工程设计有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

During the recrystallization annealing process, these alloy elements are easy to produce external oxidation in the annealing furnace, and the oxides are enriched on the surface of the steel strip, which makes the wettability of the steel plate in the zinc pot worse, causing problems such as missing plating or surface slag inclusion, that is, The traditional steel hot-dip galvanizing process is not suitable for high-strength steel galvanizing; if the electroplating process is used, there will be "three wastes" that pollute the environment, which is restricted by environmental protection regulations and greatly limited in application; so advanced high-strength steel galvanizing It is a major problem that plagues various iron and steel enterprises and scientific research institutions
In the existing experimental technology, the preparation of alloy coating usually requires the combination of PVD vacuum coating equipment and vacuum annealing furnace. After coating, the product is transferred to the annealing furnace for annealing. Coating and annealing are carried out separately. Integrated with annealing in the same unit to produce the process flow of alloyed coated steel plate, the production cycle is long and it is easy to oxidize before the alloy coating is formed

Method used

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  • Multifunctional experiment device and method for deposition of zinc alloy coating
  • Multifunctional experiment device and method for deposition of zinc alloy coating
  • Multifunctional experiment device and method for deposition of zinc alloy coating

Examples

Experimental program
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Effect test

Embodiment 1

[0033] refer to Figure 1 to Figure 3 , a multifunctional experimental device for depositing a zinc alloy coating in this embodiment, an evaporation unit 3, a magnetron sputtering unit 8 and a heating unit 7 are integrated in a coating chamber; The above three functional components are set in the space. This embodiment adopts the integrated optimization design concept, and the above three different functional components are arranged in the same coating room 1. The coating room 1 is a double-layer circulating water cooling structure, and a double-layer water cooling structure is provided. The front door 12 is opened, and the front door is provided with an external peep hole 13; in this embodiment, the vapor deposition part 3 is arranged on one side of the bottom of the coating chamber 1, and the magnetron sputtering part 8 is arranged on the two side walls of the coating chamber 1, And a plurality of heating components 7 are arranged on the top of one side of the inner wall of ...

Embodiment 2

[0039] This embodiment is a multifunctional experimental device, which is integrated with an evaporation unit 3 , a magnetron sputtering unit 8 and a heating unit 7 . Metal magnesium with a thickness of about 550nm was deposited on the hot-dip galvanized substrate DC54D+Z (an ultra-deep-drawn hot-dip galvanized steel sheet) by DC magnetron sputtering, and vacuum diffusion annealing was performed at 350°C, and the holding time was 2min, 5min and 6min respectively. , to obtain zinc-magnesium alloy coated steel plate.

[0040] 1) Put the hot-dip galvanized substrate 6 through chemical cleaning to remove the grease or dirt on the surface, put it into the multi-functional coating chamber 1 and fix it on the substrate frame 5;

[0041] 2) Turn on the compressed air, circulate the cooling water, turn on the power, turn on the vacuum pump unit 23 to evacuate to 3x10 -3 Pa;

[0042] 3) Turn on the infrared radiation heating lamp 7 to heat the substrate 6, and bake and degas the subst...

Embodiment 3

[0049] 1) The hot-dip galvanized steel sheet is chemically cleaned and ultrasonically cleaned to remove grease and dirt on the surface, put into the plating chamber 1 and fixed on the substrate frame 5;

[0050] 2) Turn on the circulating cooling water, turn on the power supply, and turn on the vacuum pump unit 23 to evacuate to 3x10- 3 Pa;

[0051] 3) Turn on the infrared radiation heating lamp 7, and heat the substrate 6 at 150°C for baking and degassing; use the Kaufman ion source 2 to clean the surface of the substrate 6 for (10-15) minutes, and the working vacuum of the Kaufman ion source (0.01-0.03) Pa;

[0052]4) Put cylindrical aluminum particles with a diameter of 3mm and a height of 3mm in the crucible 9 of the electron gun, so that the acceleration current is not greater than 20mA, the electron beam current is (1.2-2) times the ion beam current, and the value of the screen electrode voltage is ( 200-300) V, adjust the size of the electron beam spot, observe from t...

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Abstract

The invention provides a multifunctional experiment device and method for deposition of a zinc alloy coating; a vapor plating component, a magnetron sputtering component and heating components are integratedly arranged in the multifunctional experiment device; the vapor plating component is arranged on one side of the bottom of a plating chamber, the magnetron sputtering component is arranged on two side walls of the plating chamber, the heating components are arranged on the upper part of one side of the inner wall of the plating chamber; through use of the multifunctional experiment device, deposition of the alloy coating on the steel substrate surface can be realized through vapor plating and annealing or through magnetron sputtering and annealing on the same device; through use of the multifunctional experiment device, the common functions of multiple functional-components are tactfully shared in the same device, and unique functions of each functional component are respectively used; through use of the multifunctional experiment device, vacuum vapor plating + annealing or magnetron sputtering + annealing can be continuously carried out under vacuum conditions, a hidden trouble that product defects may generate in a discontinuous production process can be eliminated, and the quality and performance of an alloy coating product can be ensured; and the multifunctional experiment device has the advantages compact structure and complete functions and is material-saving and energy-saving.

Description

technical field [0001] The invention relates to physical vapor deposition technology, in particular to a multifunctional experimental device and an experimental method for preparing (Physical Vapor Deposition, PVD) zinc alloy coatings by using physical vapor deposition technology. Background technique [0002] As the most important corrosion protection product in the automotive, construction and home appliance industries, galvanized steel sheets provide corrosion protection for steel sheets. Galvanized steel sheets are affected by the lightweight of automobiles, the large-scale application of high-strength steel / advanced high-strength steel, and the shortage of zinc resources. Under the premise of ensuring the safety of the occupants, the most economical and effective way to achieve lightweight vehicles is to use high-strength steel or advanced high-strength steel on the body. Strengthening elements such as Si, Mn, and Al need to be added to advanced high-strength steels. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C14/24C23C14/35C23C14/46C23C14/14
Inventor 江社明习中革张启富袁训华李远鹏刘昕张杰
Owner 北京钢研新冶工程设计有限公司
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