Phosphorus-modified phenolic resin and preparation method thereof
A technology of phenolic resin and phosphorus modification, which is applied in the field of phosphorus-modified phenolic resin and its preparation, and achieves the effects of reducing environmental pollution, optimizing production conditions and excellent film-forming stability.
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[0021] Table 1 shows the reaction raw material components and reaction conditions in Examples 1 to 10, wherein the phenols described in Examples 1 to 10 are all nonylphenols.
[0022] Prepare according to the following preparation steps in conjunction with the reaction raw material components and reaction conditions that table 1 provides:
[0023] A. Take phenol, formaldehyde and water and add them into a four-necked flask and mix them evenly, then add a catalyst and mix them evenly, put the four-necked flask into an electric heating mantle and heat for condensation reaction to obtain a phenolic condensate, release it after cooling down, and separate it residual moisture;
[0024] B. Add the phenolic condensate obtained in step A back into the four-neck bottle, add monohydric alcohol and mix evenly, then add aluminum oxide and sulfuric acid as a catalyst, keep warm and reflux for dehydration reaction after heating up, and seal the phenolic condensate with one side terminal-ba...
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