Silver phosphate/zinc oxide composite photocatalytic material and preparation method therefor
A composite photocatalysis and zinc oxide technology, applied in the field of photocatalysis, can solve the problems of poor purification effect and high cost, and achieve the effects of less energy consumption, reduced preparation cost, and improved visible light photocatalytic effect.
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[0024] Example 1
[0025] Dissolve 150 mg of ZnO in 40 ml of deionized water for 30 minutes to obtain a ZnO dispersion; weigh 1.529 g of silver nitrate and dissolve in 20 ml of deionized water, and stir for 10 minutes to obtain a silver nitrate solution. Add dropwise to the ZnO dispersion under stirring conditions, stir for 6 hours at a rate of 100 revolutions per minute to form a mixed precursor solution A; weigh 0.426 g Na 2 HPO 4 The solid was dissolved in 20 ml of deionized water and ultrasonically dissolved to obtain a disodium hydrogen phosphate solution. The prepared disodium hydrogen phosphate solution was added dropwise to the mixed precursor solution A. The reaction system appeared brownish-yellow and turbid, and the addition was completed. The resulting mixed solution was continuously stirred for 30 minutes, and the resulting product was suction filtered, washed with absolute ethanol and deionized water, and vacuum dried.
Example Embodiment
[0026] Example 2
[0027] Dissolve 300 mg of ZnO in 40 ml of deionized water for 30 minutes to obtain a ZnO dispersion; weigh 1.529 g of silver nitrate in 20 ml of deionized water and stir for 10 minutes to obtain a silver nitrate solution. Add dropwise to the ZnO dispersion under stirring conditions, and stir for 8 hours at a rate of 100 revolutions per minute to form a mixed precursor solution A; weigh 0.426 g Na 2 HPO 4 The solid was dissolved in 20 ml of deionized water and ultrasonically dissolved to obtain a disodium hydrogen phosphate solution, and then the prepared disodium hydrogen phosphate solution was added dropwise to the mixed solution A, the reaction system appeared brownish-yellow turbidity, after the addition was completed The obtained mixed solution was continuously stirred for 40 minutes, and the obtained product was suction filtered, washed with absolute ethanol and deionized water, and dried in vacuum.
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[0028] Example 3
[0029] Dissolve 600 mg of ZnO in 40 ml of deionized water for 30 minutes to obtain a ZnO dispersion; weigh 1.529 g of silver nitrate and dissolve in 20 ml of deionized water, and stir for 10 minutes to obtain a silver nitrate solution; Add dropwise to the ZnO dispersion under stirring conditions, stir at 100 rpm for 10 hours to form a mixed precursor solution A; weigh 0.426 g Na 2 HPO 4 The solid was dissolved in 20 ml of deionized water and ultrasonically dissolved to obtain a disodium hydrogen phosphate solution, and then the prepared disodium hydrogen phosphate solution was added dropwise to the mixed solution A, the reaction system appeared brownish-yellow turbidity, after the addition was completed The obtained mixed solution was continuously stirred for 50 minutes, and the obtained product was suction filtered, washed with absolute ethanol and deionized water, and dried in vacuum.
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