Preparation method and application of tungsten sulfide quantum dot and noble metal nanoparticle co-modified bismuth oxybromide composite material
A nanoparticle and composite material technology, applied in the field of preparation of bismuth oxybromide composite materials, can solve the problems of low quantum conversion efficiency, low utilization rate of sunlight, etc., achieve degradable harmful pollutants, enhance utilization rate of sunlight and photons Efficient, easy to achieve results
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0029] The preparation steps of BiOBr samples are as follows:
[0030] Weighing 0.004mol Bi (NO 3 ) 3 ·5H 2 O (1.94g), added to a beaker containing 40mL of ethylene glycol and stirred for 30 minutes, then the molar ratio was: Bi(NO 3 ) 3 ·5H 2 O:KBr=1:1, add 0.004mol KBr (0.476g) and continue stirring for 30 minutes, the obtained reaction solution is transferred to a stainless steel reaction kettle lined with polytetrafluoroethylene, and kept at 140° C. for 24 hours. The obtained product was washed with absolute ethanol and deionized water, and the final product was dried in an oven at 80 °C for 12 hours to obtain a BiOBr sample. The degradation efficiency of the product in this example under visible light for 30 minutes to the dye Rhodamine B (RhB) was 63.5%, the degradation efficiency of RhB for 60 minutes was 76.4%, and the degradation efficiency of RhB for 90 minutes was 83.2%.
[0031] WS 2 The preparation steps of quantum dot samples are as follows:
[0032] Take...
Example Embodiment
[0033] Example 1
[0034] Weigh 2g BiOBr sample, add 250mL deionized water to ultrasonic for 1 hour, add 0.032g AgNO according to 1wt% Ag / BiOBr 3 Stir at 35°C for 3h under oil bath condition, then warm up to 95°C, add 0.022g NaBH 4 Cool to room temperature after half an hour. The resulting product was isolated, washed and dried to obtain a BiOBr catalyst supported by precious metal Ag nanoparticles (labeled as 1% Ag / BiOBr). The degradation efficiency of RhB under visible light for 90 minutes by the product of this example is 94.2%, which is 1.13 times that of pure BiOBr.
Example Embodiment
[0035] Example 2
[0036] Weigh 2g BiOBr sample, add 250mL deionized water for 1 hour, add 0.04g chloroauric acid according to 1wt% Au / BiOBr, stir at 35°C for 3h under oil bath conditions, then heat up to 95°C, add 0.012g NaBH 4 Cool to room temperature after half an hour. The resulting product was isolated, washed and dried to obtain a BiOBr catalyst supported by precious metal Au nanoparticles (labeled as 1% Au / BiOBr). The degradation efficiency of RhB by the product of this example under visible light for 90 minutes is 88.2%, which is 1.06 times that of pure BiOBr.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap