The invention discloses a compounding method for a nanometer ultrathin 
boron carbon nitrogen sheet and belongs to the technical field of material preparation. The method comprises the following steps: mixing diboron 
trioxide, 
melamine, glucose and the mixed salt of NaCl and KCL, then 
grinding, and performing heat treatment on the acquired 
powder under the 
atmosphere of 
ammonia gas, thereby acquiring the nanometer ultrathin 
boron carbon nitrogen sheet. According to the invention, the low-cost mixed salt and the 
boron carbon nitrogen precursor have a heating reaction under the 
atmosphere of 
ammonia gas, and the fused mixed salt is utilized as a template of the boron carbon 
nitrogen sheet, is evaporated at high temperature and is peeled, so that the nanometer ultrathin boron carbon 
nitrogen sheet characterized by having a 
graphite like phase 
crystal structure, the thickness of an atom-level ultrathin sheet, a huge size and a high specific area can be prepared. The compounding method disclosed by the invention is simple in operation; complex and expensive instruments and equipment are not required; the adopted raw materials are low in cost and are easily acquired; the environmental 
pollution is little; the method is suitable for large-scale production; and the compounding method has significance in boosting the application of the nanometer ultrathin boron carbon 
nitrogen sheet in the fields of photoelectric materials, organic 
catalysis, 
hydrogen storage carriers, detection analysis, and the like.