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A method of series/parallel adjustable ultrasonic tank demulsification

An ultrasonic and demulsification technology, which is applied in the direction of electric/magnetic dehydration/demulsification, immiscible liquid separation, chemical/physical/physicochemical process of energy application, etc., can solve the problems of electroacoustic efficiency, high manufacturing cost, Problems such as complex equipment structure, to achieve the effect of prolonging the action time

Active Publication Date: 2015-08-19
CHINA PETROLEUM & CHEM CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Over the years, the research on crude oil demulsification technology is mostly limited to the research of chemical demulsifiers, which has great limitations on different types of crude oil, and the application of demulsifiers has many production and environmental problems: resulting in increased production costs, resulting in The oil content and COD value of the drainage will increase, which will directly affect the normal operation and standard discharge of subsequent sewage treatment
Its device directly refits the raw material storage tank or settling tank. Since the upper head of the raw material storage tank or settling tank is a convex structure, its defect is that it takes a long time for the ultrasonic transducer to extend into the ultrasonic demulsification tank. The length of the rod directly affects the electroacoustic efficiency, and the ultrasonic waves generated by the ultrasonic distributor cannot effectively affect the oil-water emulsion; when the device is used, the raw material storage tank or the settling tank needs to be temporarily refitted to install multiple ultrasonic generators
The ultrasonic distributor directly acts on the oil-water emulsion to cause dead angle or short circuit phenomenon. The equipment structure is complicated, the inspection and maintenance are inconvenient, the manufacturing cost is high, and the reusability is poor.

Method used

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  • A method of series/parallel adjustable ultrasonic tank demulsification
  • A method of series/parallel adjustable ultrasonic tank demulsification

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] Such as figure 2 As shown, the ultrasonic demulsification tanks and the sedimentation dehydration tanks 13 are connected by pipelines, and the fourth valve 4, the fifth valve 5, the sixth valve 6, the seventh valve 7, the eighth valve 8, and the fourth valve are arranged between the pipelines. Nine valves 9 and tenth valves 10 are used to adjust the series-parallel relationship between the two ultrasonic demulsification tanks. Close the fifth valve 5 and the eighth valve 8, open the fourth valve 4, the sixth valve 6, the seventh valve 7, the ninth valve 9, and the tenth valve 10, which can realize single-stage parallel operation, suitable for different emulsification degrees Demulsification of oil-water emulsion; open the fifth valve 5, the eighth valve 8, close the fourth valve 4, the sixth valve 6, the seventh valve 7, and the ninth valve 9, which can realize 3-stage series operation, and choose to pass through 3 stages step by step Stage series demulsification, sui...

Embodiment 2

[0045] The device described in Example 1 was used.

[0046] Such as figure 2 As shown, before the crude oil enters the tank, enter the device installed in series / parallel of the above three ultrasonic demulsification tanks, conduct the ultrasonic tank demulsification test of high water content Shengli crude oil, open the fifth valve 5, the eighth valve 8, and close the fourth The valve 4, the sixth valve 6, the seventh valve 7, and the ninth valve 9 realize series operation. The speed of water-containing crude oil through the total feed port is 2m 3 / min. After the tank-type demulsification of three ultrasonic demulsification tanks connected in series with a single set of ultrasonic transducers and distributors, the emulsified waste oil with high water content is subjected to sedimentation and dehydration for 48 hours in the sedimentation dehydration tank. The temperature in the ultrasonic demulsification tank is controlled to be 85°C, the ultrasonic frequency is 160kHz in...

Embodiment 3

[0048] The device described in Example 1 was used.

[0049] Such as figure 2 As shown, before the crude oil enters the tank, it enters the above-mentioned three ultrasonic demulsification tanks installed in series / parallel to perform ultrasonic tank demulsification of high water content Shengli crude oil, close the fifth valve 5 and the eighth valve 8, and open the fourth valve 4. The sixth valve 6, the seventh valve 7, the ninth valve 9, and the tenth valve 10 realize the parallel operation of three ultrasonic demulsification tanks. The speed of water-containing crude oil through the total feed port is 4m 3 / min. After the tank-type demulsification of three ultrasonic demulsification tanks in parallel with a single set of ultrasonic transducers and distributors, the emulsified oil with high water content is subjected to sedimentation and dehydration in the sedimentation dehydration tank for 48 hours. Control the temperature in the ultrasonic demulsification tank to 20°C, ...

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Abstract

The invention discloses a serial / parallel connection adjustable ultrasonic wave tank type demulsification method. At least two ultrasonic demulsification tanks are connected in series / in parallel to an intermediate pipeline of an oil-water emulsion storage tank or a pipeline before an oil-water emulsion enters the tank, one set of ultrasonic transduction distribution devices is arranged, an ultrasonic distributor is arranged in an ultrasonic demulsification tank and is connected with the ultrasonic demulsification tank through a pipeline, a fully-serial connection, fully-parallel connection or parallel-connection and serial-connection jointed any-transformation ultrasonic demulsification function is realized by regulation of a valve, and thus the oil-water emulsion is dewatered. The device and method are multi functional, convenient to install and simple in internal structure, are suitable for tank type demulsification and dewatering in an oil field or oil refinery, and particularly suitable for complicated and variable occasions with multifunctional requirements of needing multiple stages of serial connection and parallel connection for prolonging ultrasonic wave acting time or a parallel connection-serial connection joint function for the oil-water emulsion.

Description

technical field [0001] The invention discloses a series / parallel adjustable ultrasonic tank-type demulsification method, which belongs to the field of petrochemical technical equipment. Background technique [0002] In recent years, with the gradual reduction of petroleum resources and the continuous increase of people's demand for petroleum products, oilfield companies have been prompted to adopt various measures to increase production, using crude oil reserves that were difficult to exploit in the past, and widely applying tertiary oil recovery technologies, such as polymer flooding, multi-component compounding, etc. The extensive application of technologies such as flooding, surface active flooding, alkali flooding, carbon dioxide flooding, and thermal recovery of heavy oil has resulted in intensified emulsification of heavy and inferior crude oil and stable emulsified structure. It is difficult to quickly achieve effective emulsification by traditional thermochemical mean...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D17/04B01J19/10C10G33/02
Inventor 苟社全常文之张红宇许金山刘爱华张传明王建华梁颖杰崔云梓
Owner CHINA PETROLEUM & CHEM CORP
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