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O/W (oil in water) type lemon essential oil containing sub-micron emulsion and preparation method thereof

A technology of oil submicron, lemon essential oil, applied in the chemical field, can solve the problems of uneven particle size, difficult penetration, poor stability, etc., and achieve the effects of good skin feel, reduced irritation, and good stability

Active Publication Date: 2015-07-22
FOSHAN WIN COSMETIC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Aiming at the above-mentioned defects existing in the prior art, the technical problem to be solved by the present invention is to provide a kind of O / W type containing lemon essential oil submicron emulsion and preparation method thereof, said O / W type containing lemon essential oil The sub-micron emulsion and its preparation method solve the above-mentioned technical problems such as lemon essential oil directly acting on human skin to cause certain irritation, ordinary emulsion emulsified particle size is uneven, large particle size, poor stability, and difficult to penetrate.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] An O / W type submicron emulsion containing lemon essential oil, calculated by weight percentage, the composition and content of each raw material in the described O / W type submicron emulsion containing lemon essential oil are as follows:

[0050] Lemon Essential Oil 5%

[0051] Liquid grease 1%

[0052] Liquid emulsifier 3%

[0053]Organic additives 1%

[0054] Inorganic additives 0.01%

[0055] Water 89.99%

[0056] Described lemon essential oil, the food-grade product of Shanghai IKEA Spice and Flavor Co., Ltd.;

[0057] The liquid oil is caprylic acid / capric triglyceride, a cosmetic grade product of Croda Chemicals (Shanghai) Co., Ltd.;

[0058] Described liquid emulsifier is sorbitan fatty acid ester and polyoxyethylene sorbitan fatty acid

[0059] Composition of the mixture, wherein sorbitan fatty acid ester 1%, polyoxyethylene sorbitan fatty acid ester 2%, the HLB value of the mixture is 11.43, wherein the sorbitan fatty acid ester is 1%, and the HLB value is...

Embodiment 2

[0067] An O / W type submicron emulsion containing lemon essential oil, calculated by weight percentage, the composition and content of each raw material in the described O / W type submicron emulsion containing lemon essential oil are as follows:

[0068] Lemon Essential Oil 17.5%

[0069] Liquid Grease 10%

[0070] Liquid Emulsifier 14%

[0071] Organic additives 7.5%

[0072] Inorganic additives 0.5%

[0073] Water 50.5%

[0074] Described lemon essential oil, the food-grade product of Shanghai IKEA Spice and Flavor Co., Ltd.;

[0075] The liquid oil is macadamia nut oil, a cosmetic grade product of Laibaokang Daily Chemical (Shanghai) Co., Ltd.;

[0076] The liquid emulsifier is a mixture of caprylic / capric macrogol glyceride and polyglycerol-3-diisostearate 5.5, and the HLB value of the mixture is 10.29, wherein caprylic / capric macrogol Glyceride 8%, HLB value 14, polyglyceryl-3-diisostearate 4%, HLB value 5.5, cosmetic grade product of Jiafashi (Shanghai) Trading Co., ...

Embodiment 3

[0084] An O / W type submicron emulsion containing lemon essential oil, calculated by weight percentage, the composition and content of each raw material in the described O / W type submicron emulsion containing lemon essential oil are as follows:

[0085] Lemon Essential Oil 30%

[0086] Liquid Grease 20%

[0087] Liquid emulsifier 20%

[0088] Organic additives 15%

[0089] Inorganic additives 1.0%

[0090] water 14%

[0091] Described lemon essential oil, the food-grade product of Shanghai IKEA Spice and Flavor Co., Ltd.;

[0092] The liquid oil is jojoba oil, a cosmetic grade product of Laibaokang Daily Chemical (Shanghai) Co., Ltd.;

[0093] Described liquid emulsifier is laureth-7, and its physical state of laureth emulsifier is changed from liquid to semi-solid and then becomes solid with the increase of EO number, and HLB value also increases with the increase of EO number. Increase, where EO ≤ 7 is liquid, EO ≤ 15 is semi-solid, EO ≥ 15 is solid, the content of laur...

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PUM

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Abstract

The invention provides an O / W (oil in water) type lemon essential oil containing submicron emulsion. The emulsion comprises the following components in percentage by weight: 5-30 percent of lemon essential oil, 1-20 percent of liquid fat, 3-20 percent of liquid emulsifying agent, 1-15 percent of organic additive, 0.01-2.0 percent of inorganic additive, and the balance of water. The invention also provides a preparation method of the submicron emulsion, and the preparation method comprises the following steps: mixing the lemon essential oil, the liquid fat and the emulsifying agent to obtain a uniform oil phase component; mixing the organic additive, the inorganic additive and the water to obtain an aqueous phase component; adding the oil phase component into the aqueous phase component by utilizing a cooling preparation method, stirring to form a coarse emulsion, and performing high-pressure homogenization on the coarse emulsion to obtain the submicron emulsion. According to the submicron emulsion, the coarse emulsion is prepared by utilizing a cooling preparation method and subjected to high-pressure homogenization to obtain the submicron emulsion, and the submicron emulsion which has uniform and smaller dispersed phase particle diameter and contains lemon essential oil is formed in the phase inversion process, so that irritation of the lemon essential oil by directly acting on the skin can be reduced.

Description

technical field [0001] The invention belongs to the field of chemical industry, and in particular relates to a cosmetic and a preparation method thereof, in particular to an O / W type submicron emulsion containing lemon essential oil and a preparation method thereof. Background technique [0002] Lemon essential oil comes from lemon fruit and peel, and lemon essential oil is obtained by steam distillation, cold pressing or cold grinding process. Lemon essential oil is composed of a variety of volatile components, mainly monoterpenes and carbohydrates, which give us a fresh, natural and pleasant fruity aroma. Lemon essential oil has been used as essence in food, beverage, wine and confectionary industries, and also used in daily chemical industry soap and perfume flavoring agent. At the same time, many lemon essential oil products are used in aromatherapy to make people work after high intensity Yu complacently relaxes. Today's scientific research on lemon essential oil main...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K8/97A61K8/92A61K8/06A61Q19/00A61Q19/02A61Q13/00
Inventor 张婉萍胡君姣陈良红刘晓慧
Owner FOSHAN WIN COSMETIC
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