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Compound Ilex purpurea hassk ointment as well as preparation method and detection method thereof

A detection method, the technology of green ointment, which is applied in ointment delivery, pharmaceutical formula, color/spectral characteristic measurement, etc., can solve the problem that the purple handle holly ointment does not have strict and reliable quality inspection standards, etc.

Inactive Publication Date: 2014-04-23
涂金兰
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, there is no strict, reliable and complete quality inspection standard for Zishan Dongqing Ointment

Method used

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  • Compound Ilex purpurea hassk ointment as well as preparation method and detection method thereof
  • Compound Ilex purpurea hassk ointment as well as preparation method and detection method thereof
  • Compound Ilex purpurea hassk ointment as well as preparation method and detection method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0099] Embodiment 1: A kind of compound Sijiqing ointment is made of Sijiqing 100g, rhubarb 80g, comfrey 60g, honeysuckle 40g, corydalis 20g, borneol 4g and yellow vaseline 1000g.

[0100] The preparation method of this compound Sijiqing ointment: first weigh 200g of yellow vaseline and heat and melt, add comfrey 60g and decoct with slow fire for 1 hour, filter with 4 layers of gauze, and keep the filtrate and residue for later use; then heat and melt 800g of yellow vaseline, add Fry 80g of rhubarb and 20g of Corydalis corydalis until browned, then add 40g of honeysuckle, 100g of Sijiqing and comfrey residue and fry for 1 hour, filter with 4 layers of gauze, combine the two filtrates, add 4g of borneol after cooling slightly, stir to make It is completely dissolved, allowed to cool, and packaged separately to obtain Compound Sijiqing Ointment.

Embodiment 2

[0101] Embodiment 2: the method for assaying the content of L-shikonin contained in Shicao in the obtained compound Sijiqing ointment of embodiment 1, specifically comprises the following steps:

[0102] ①Preparation of reference substance solution: Accurately weigh (1 / 100,000 balance) 5.04mg of levoshikonin reference substance, put it in a 50mL measuring bottle, add ethanol to dissolve and dilute to the mark, shake well, and use it as the reference substance solution;

[0103] ②Preparation of the test solution: Weigh 5g of this preparation, put it in a small beaker, add 5g of diatomaceous earth, stir well, transfer it to a stoppered Erlenmeyer flask, add 100mL of ethanol, put it in a water bath at 50°C for 40min, and put Cool, let it stand, filter, and accurately measure 5 mL of the filtrate to a 25 mL measuring bottle, add ethanol to the mark, shake well, and use it as the test solution;

[0104] ③Drawing of the standard curve: Accurately draw reference substance solutions 1...

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PUM

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Abstract

The invention provides a compound Ilex purpurea hassk ointment as well as a preparation method and a detection method thereof. The compound Ilex purpurea hassk ointment is made from 100 g of Ilex purpurea hassk, 80 g of rhubarb, 60 g of lithospermum, 40 g of honeysuckle, 20 g of rhizoma corydalis, 4 g of borneol and 1000 g of yellow Vaseline. Aiming at the defects of the prior art, the preparation process of the compound Ilex purpurea hassk ointment is optimized to ensure better curative effects of clearing away heat and toxic materials, relieving swelling and pain, astringing and promoting regeneration of tissue, a content measurement method of L-shikonin contained in the monarch drug lithospermum is established, and is high in precision, good in accuracy and capable of effectively controlling the quality of the medicine, thereby ensuring the clinical curative effect of the medicine.

Description

technical field [0001] The invention relates to a compound Sijiqing ointment, a preparation method and a detection method thereof, and belongs to the technical field of traditional Chinese medicines. Background technique [0002] Purple handle holly ointment is made of purple handle holly, comfrey, rhubarb, silver flower, borneol and corydalis as raw materials. Good application effects have been achieved in the healing of infected wounds and ulcers. [0003] The traditional preparation process of Zishan Dongqing ointment is as follows: first weigh 1000g of yellow vaseline, heat and melt, add 60g of comfrey and fry it with a slow fire for 1 hour, add 80g of rhubarb and 20g of Corydalis, fry until it is browned, and then add 40g of honeysuckle 1. Fry 100g of Ilex chinensis with slow fire for 1 hour, filter with 4 layers of gauze, add 4g of borneol after a little cooling, stir to make it completely dissolve, let it cool, and pack it separately to get ready. In the preparation...

Claims

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Application Information

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IPC IPC(8): A61K36/80A61K36/708A61K9/06A61P17/02G01N21/31A61K31/045
Inventor 涂金兰
Owner 涂金兰
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